C₅₅H₇₄O₉Si

Base Information

Chemical Name:C₅₅H₇₄O₉Si
CAS No.:927662-04-2
Molecular Formula:C₅₅H₇₄O₉Si
Molecular Weight:907.273
Hs Code.:

C<sub>55</sub>H<sub>74</sub>O<sub>9</sub>Si

Synonyms:C₅₅H₇₄O₉Si

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Chemical Property of C₅₅H₇₄O₉Si

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Technology Process of C₅₅H₇₄O₉Si

There total 12 articles about C₅₅H₇₄O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 927662-03-1
C₅₃H₇₀O₉Si

: 1112-56-7
tetravinyltin (IV)

: 927662-04-2
C₅₅H₇₄O₉Si

Guidance literature:: With methyllithium; In tetrahydrofuran; at -78 - 20 ℃; for 1h;
DOI:10.3987/COM-06-S(O)23

Reference yield:

: 927661-98-1
C₃₁H₄₅NO₄Si

: 927662-04-2
C₅₅H₇₄O₉Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: DIBAL-H / CH₂Cl₂ / -78 °C

1.2: NaBH₄ / ethanol / 1.5 h / 20 °C

1.3: 78 percent / TBAF / tetrahydrofuran / 1 h / 20 °C

2.1: 78 percent / Sc(OTf)3 / benzene / 14 h / 20 °C

3.1: Sc(OTf)3 / CH₂Cl₂ / 9.5 h / 20 °C

3.2: 92 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

4.1: 2-nitrobenzeneselenide; Bu₃P / tetrahydrofuran / 0.42 h / 20 °C

4.2: 77 percent / H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 3.5 h / 45 °C

5.1: 89 percent / DIBAL-H / CH₂Cl₂ / 0.5 h / -78 °C

6.1: 76 percent / MeLi / tetrahydrofuran / 1 h / -78 - 20 °C

With tributylphosphine; methyllithium; diisobutylaluminium hydride; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; dichloromethane; benzene;
DOI:10.3987/COM-06-S(O)23

Reference yield:

: 927661-96-9
C₂₇H₃₈O₄Si

: 927662-04-2
C₅₅H₇₄O₉Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 9-BBN / tetrahydrofuran / 3 h / 20 °C / sonication

1.2: H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 1 h / 20 °C

1.3: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.58 h / 20 °C

2.1: 78 percent / Sc(OTf)3 / benzene / 14 h / 20 °C

3.1: Sc(OTf)3 / CH₂Cl₂ / 9.5 h / 20 °C

3.2: 92 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

4.1: 2-nitrobenzeneselenide; Bu₃P / tetrahydrofuran / 0.42 h / 20 °C

4.2: 77 percent / H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 3.5 h / 45 °C

5.1: 89 percent / DIBAL-H / CH₂Cl₂ / 0.5 h / -78 °C

6.1: 76 percent / MeLi / tetrahydrofuran / 1 h / -78 - 20 °C

With 9-borabicyclo[3.3.1]nonane dimer; tributylphosphine; methyllithium; diisobutylaluminium hydride; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; dichloromethane; benzene;
DOI:10.3987/COM-06-S(O)23