1,4-Bis-(2-hydroxy-4,6-dimethoxy-phenyl)-2,3-bis-(4-methoxy-benzoyl)-butane-1,4-dione

Base Information

Chemical Name:1,4-Bis-(2-hydroxy-4,6-dimethoxy-phenyl)-2,3-bis-(4-methoxy-benzoyl)-butane-1,4-dione
CAS No.:120341-55-1
Molecular Formula:C₃₆H₃₄O₁₂
Molecular Weight:658.659
Hs Code.:

Synonyms:1,4-Bis-(2-hydroxy-4,6-dimethoxy-phenyl)-2,3-bis-(4-methoxy-benzoyl)-butane-1,4-dione

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Chemical Property of 1,4-Bis-(2-hydroxy-4,6-dimethoxy-phenyl)-2,3-bis-(4-methoxy-benzoyl)-butane-1,4-dione

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Technology Process of 1,4-Bis-(2-hydroxy-4,6-dimethoxy-phenyl)-2,3-bis-(4-methoxy-benzoyl)-butane-1,4-dione

There total 4 articles about 1,4-Bis-(2-hydroxy-4,6-dimethoxy-phenyl)-2,3-bis-(4-methoxy-benzoyl)-butane-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 120341-54-0
C₃₆H₃₄O₁₂

: 120341-55-1
1,4-Bis-(2-hydroxy-4,6-dimethoxy-phenyl)-2,3-bis-(4-methoxy-benzoyl)-butane-1,4-dione

Guidance literature:: With sodium hydride; In toluene;
DOI:10.1039/c39880001549

Reference yield:

: 621-23-8
1,2,3-trimethoxybenzene

: 120341-55-1
1,4-Bis-(2-hydroxy-4,6-dimethoxy-phenyl)-2,3-bis-(4-methoxy-benzoyl)-butane-1,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / AlCl₃ / various solvent(s)

2: 98 percent / BCl₃ / CH₂Cl₂

3: 81 percent / pyridine

4: 89 percent / NaH / toluene

With pyridine; aluminium trichloride; boron trichloride; sodium hydride; In dichloromethane; toluene;
DOI:10.1039/c39880001549

Reference yield:

: 120341-52-8
1,4-Bis-(2-hydroxy-4,6-dimethoxy-phenyl)-butane-1,4-dione

: 120341-55-1
1,4-Bis-(2-hydroxy-4,6-dimethoxy-phenyl)-2,3-bis-(4-methoxy-benzoyl)-butane-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / pyridine

2: 89 percent / NaH / toluene

With pyridine; sodium hydride; In toluene;
DOI:10.1039/c39880001549