1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene

Base Information

Chemical Name:1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene
CAS No.:1236189-75-5
Molecular Formula:C₂₀H₃₄O₉P₂
Molecular Weight:480.432
Hs Code.:

Synonyms:1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene

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Chemical Property of 1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene

There total 7 articles about 1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₄₀O₁₀P₂

: 1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene

: 1236189-75-5
1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene

: C₂₄H₄₀O₁₀P₂

: 1,4-di[(diethoxyphosphoryl)hydroxymethyl]benzene

: C₂₄H₄₀O₁₀P₂

Guidance literature:: With lipase from Candida cylindracea; In aq. phosphate buffer; hexane; at 20 ℃; for 24h; stereospecific reaction; Enzymatic reaction;
DOI:10.3998/ark.5550190.0013.422

Reference yield:

: C₂₄H₄₀O₁₀P₂

: 1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene

: 1236189-75-5
1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene

: C₂₄H₄₀O₁₀P₂

: 1,4-di[(diethoxyphosphoryl)hydroxymethyl]benzene

: 1,4-di[(diethoxyphosphoryl)hydroxymethyl]benzene

: C₂₄H₄₀O₁₀P₂

Guidance literature:: With lipase from Candida cylindracea; In aq. phosphate buffer; hexane; at 20 ℃; for 168h; stereospecific reaction; Enzymatic reaction;
DOI:10.3998/ark.5550190.0013.422

Reference yield:

: 623-27-8
terephthalaldehyde,

: 1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene

: 1236189-75-5
1-[(diethoxyphosphoryl)butyryloxymethyl]-4-[(diethoxyphosphoryl)hydroxymethyl]benzene

: C₂₄H₄₀O₁₀P₂

: 1,4-di[(diethoxyphosphoryl)hydroxymethyl]benzene

: C₂₄H₄₀O₁₀P₂

Guidance literature:: Multi-step reaction with 3 steps

1: potassium fluoride; aluminum oxide / 12 h / 20 °C

2: triethylamine / chloroform / 8 h / 0 °C / Reflux

3: lipase from Candida cylindracea / hexane; aq. phosphate buffer / 24 h / 20 °C / Enzymatic reaction

With aluminum oxide; potassium fluoride; lipase from Candida cylindracea; triethylamine; In aq. phosphate buffer; hexane; chloroform;
DOI:10.3998/ark.5550190.0013.422