methyl 5-(2-(4-bromophenyl)-2-chloroethyl)-3-(3-chloropropyl)-4,6-dimethylsalicylate

Base Information

Chemical Name:methyl 5-(2-(4-bromophenyl)-2-chloroethyl)-3-(3-chloropropyl)-4,6-dimethylsalicylate
CAS No.:1239709-84-2
Molecular Formula:C₂₁H₂₃BrCl₂O₃
Molecular Weight:474.222
Hs Code.:

Synonyms:methyl 5-(2-(4-bromophenyl)-2-chloroethyl)-3-(3-chloropropyl)-4,6-dimethylsalicylate

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Chemical Property of methyl 5-(2-(4-bromophenyl)-2-chloroethyl)-3-(3-chloropropyl)-4,6-dimethylsalicylate

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Technology Process of methyl 5-(2-(4-bromophenyl)-2-chloroethyl)-3-(3-chloropropyl)-4,6-dimethylsalicylate

There total 1 articles about methyl 5-(2-(4-bromophenyl)-2-chloroethyl)-3-(3-chloropropyl)-4,6-dimethylsalicylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1067232-95-4
1-[5-(4-bromophenyl)-2-methyl-4,5-dihydrofuran-3-yl]ethanone

: 1071146-53-6
7-chloro-1-methoxy-1,3-bis(trimethylsilyloxy)-1,3-heptadiene

: 1239709-84-2
methyl 5-(2-(4-bromophenyl)-2-chloroethyl)-3-(3-chloropropyl)-4,6-dimethylsalicylate

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -78 - 20 ℃; for 16h; regioselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201000158

Reference yield: 76.0%

: 1239709-84-2
methyl 5-(2-(4-bromophenyl)-2-chloroethyl)-3-(3-chloropropyl)-4,6-dimethylsalicylate

: 1239710-24-7
methyl 6-[(E)-2-(4-bromophenyl)vinyl]-5,7-dimethylchromane-8-carboxylate

Guidance literature:: methyl 5-(2-(4-bromophenyl)-2-chloroethyl)-3-(3-chloropropyl)-4,6-dimethylsalicylate; With tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; at -78 ℃; Inert atmosphere;

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;
DOI:10.1002/ejoc.201000158