1-(CHLORODIFLUOROMETHYL)-4-(DICHLOROFLUOROMETHYL)BENZENE

Base Information

• Chemical Name: 1-(CHLORODIFLUOROMETHYL)-4-(DICHLOROFLUOROMETHYL)BENZENE
• CAS No.: 13947-95-0
• Molecular Formula: C8H4 Cl3 F3
• Molecular Weight: 263.474
• Hs Code.: 2903999090
• Mol file: 13947-95-0.mol

Synonyms:p-Xylene, a,a,a'-trichloro-a,a',a'-trifluoro- (8CI)

Chemical Property of 1-(CHLORODIFLUOROMETHYL)-4-(DICHLOROFLUOROMETHYL)BENZENE

Chemical Property:

• Vapor Pressure: 0.0545mmHg at 25°C
• Refractive Index: 1.488
• Boiling Point: 241.9°Cat760mmHg
• Flash Point: 115.5°C
• PSA: 0.00000
• Density: 1.511g/cm³
• LogP: 4.53210

Purity/Quality:

97% ^*data from raw suppliers

1-(Chlorodifluoromethyl)-4-(dichlorofluoromethyl)benzene ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(CHLORODIFLUOROMETHYL)-4-(DICHLOROFLUOROMETHYL)BENZENE

There total 2 articles about 1-(CHLORODIFLUOROMETHYL)-4-(DICHLOROFLUOROMETHYL)BENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.3%

1,4-bis(trichloromethyl)benzene (68-36-0) → 1-(chlorodifluoromethyl)-4-(trifluoromethyl)benzene (13947-94-9) + 1,4-bis-(difluorochloromethyl)-benzene (2629-68-7) + 1-fluorodichloromethyl-4-difluorochloromethyl-benzene (13947-95-0)

Guidance literature:

With hydrogen fluoride; In 1,2-dichloro-ethane; at 45 ℃; for 10h; under 2280.15 Torr;

DOI:10.1016/j.jfluchem.2007.05.007

Reference yield:

→ 1-fluorodichloromethyl-4-difluorochloromethyl-benzene (13947-95-0)

Guidance literature:

4-Trichlormethyl-benzotrichlorid;

upstream raw materials:

1,4-bis(trichloromethyl)benzene

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