C₂₇H₂₆N₂O₄S₂

Base Information

Chemical Name:C₂₇H₂₆N₂O₄S₂
CAS No.:1407518-03-9
Molecular Formula:C₂₇H₂₆N₂O₄S₂
Molecular Weight:506.646
Hs Code.:

C<sub>27</sub>H<sub>26</sub>N<sub>2</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:C₂₇H₂₆N₂O₄S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₆N₂O₄S₂

Chemical Property:

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Technology Process of C₂₇H₂₆N₂O₄S₂

There total 5 articles about C₂₇H₂₆N₂O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1407518-27-7
C₂₇H₂₆N₂O₄S₂

: 1407518-03-9
C₂₇H₂₆N₂O₄S₂

Guidance literature:: With silver hexafluoroantimonate; C₂₇H₃₇AuClN₂; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol302743k

Reference yield:

: 122284-60-0
5-methyl-N-tosylindole-3-carboxaldehyde

: 1407518-03-9
C₂₇H₂₆N₂O₄S₂

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2: dmap / acetonitrile / 4 h / 0 °C / Inert atmosphere

3: potassium carbonate; [RhCl(PPh₃)3]; phosphorous acid trimethyl ester / tetrahydrofuran / 24 h / 30 °C / Inert atmosphere

4: potassium tert-butylate / tetrahydrofuran / 20 °C / Inert atmosphere

5: silver hexafluoroantimonate; C₂₇H₃₇AuClN₂ / dichloromethane / 1 h / 20 °C / Inert atmosphere

With dmap; silver hexafluoroantimonate; C₂₇H₃₇AuClN₂; [RhCl(PPh₃)3]; potassium tert-butylate; potassium carbonate; phosphorous acid trimethyl ester; In tetrahydrofuran; dichloromethane; acetonitrile; 5: |Nazarov Cyclization;
DOI:10.1021/ol302743k

Reference yield:

: 1407518-93-7
C₂₇H₂₆N₂O₄S₂

: 1407518-03-9
C₂₇H₂₆N₂O₄S₂

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 20 °C / Inert atmosphere

2: silver hexafluoroantimonate; C₂₇H₃₇AuClN₂ / dichloromethane / 1 h / 20 °C / Inert atmosphere

With silver hexafluoroantimonate; C₂₇H₃₇AuClN₂; potassium tert-butylate; In tetrahydrofuran; dichloromethane; 2: |Nazarov Cyclization;
DOI:10.1021/ol302743k