Technology Process of C29H34ClIO10
There total 8 articles about C29H34ClIO10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
dichloromethane;
at 20 ℃;
for 3h;
Overall yield = 204 mg;
DOI:10.1021/ja5013307
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine hydrogenfluoride / acetonitrile / 2 h / 20 °C
2: toluene-4-sulfonic acid / dichloromethane / 3 h / 20 °C
With
toluene-4-sulfonic acid; pyridine hydrogenfluoride;
In
dichloromethane; acetonitrile;
DOI:10.1021/ja5013307
- Guidance literature:
-
Multi-step reaction with 8 steps
1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 20 °C
2: C14H20N2O4S; chromium dichloride; lithium chloride; NiCl2*2,9-dimethyl-1,10-phenanthroline complex; manganese / acetonitrile / 20 h / 20 °C / Glovebox
3: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1 h / 20 °C
4: pyridine hydrogenfluoride; pyridine / acetonitrile / 16 h / 20 °C
5: 3,3-dimethyldioxirane / acetone / 1 h / 0 °C
6: camphor-10-sulfonic acid / dichloromethane / 0.17 h / 20 °C
7: pyridine hydrogenfluoride / acetonitrile / 2 h / 20 °C
8: toluene-4-sulfonic acid / dichloromethane / 3 h / 20 °C
With
pyridine; chromium dichloride; manganese; C14H20N2O4S; camphor-10-sulfonic acid; NiCl2*2,9-dimethyl-1,10-phenanthroline complex; 3,3-dimethyldioxirane; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; pyridine hydrogenfluoride; lithium chloride;
In
dichloromethane; acetone; acetonitrile;
DOI:10.1021/ja5013307
