5-(3-bromo-4-fluorophenyl)-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrole 1-oxide

Base Information

Chemical Name:5-(3-bromo-4-fluorophenyl)-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrole 1-oxide
CAS No.:1364921-33-4
Molecular Formula:C₁₇H₉BrCl₃F₄NO
Molecular Weight:505.521
Hs Code.:

Synonyms:5-(3-bromo-4-fluorophenyl)-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrole 1-oxide

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Chemical Property of 5-(3-bromo-4-fluorophenyl)-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrole 1-oxide

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Technology Process of 5-(3-bromo-4-fluorophenyl)-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrole 1-oxide

There total 4 articles about 5-(3-bromo-4-fluorophenyl)-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrole 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338926-74-1
1-(3-bromo-4-fluorophenyl)-4,4,4-trifluoro-3-(nitromethyl)-3-(3,4,5-trichlorophenyl)-butan-1-one

: 1364921-33-4
5-(3-bromo-4-fluorophenyl)-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrole 1-oxide

Guidance literature:: With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In 1,4-dioxane; methanol; for 1h; Inert atmosphere; Cooling with ice;

Reference yield:

: 1007-15-4
4-fluoro-3-bromoacetophenone

: 1364921-33-4
5-(3-bromo-4-fluorophenyl)-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrole 1-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydride / tetrahydrofuran / 8 h / Reflux

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 10 h / 20 °C

3: sodium tetrahydroborate; nickel(II) chloride hexahydrate / 1,4-dioxane; methanol / 1 h / Inert atmosphere; Cooling with ice

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; lithium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; 1,4-dioxane; methanol; acetonitrile;

Reference yield:

: 158401-00-4
1-(3,4,5-trichloro-phenyl)-2,2,2-trifluoro-ethanone

: 1364921-33-4
5-(3-bromo-4-fluorophenyl)-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrole 1-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydride / tetrahydrofuran / 8 h / Reflux

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 10 h / 20 °C

3: sodium tetrahydroborate; nickel(II) chloride hexahydrate / 1,4-dioxane; methanol / 1 h / Inert atmosphere; Cooling with ice

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; lithium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; 1,4-dioxane; methanol; acetonitrile;