2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-α-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-D-glucal

Base Information

• Chemical Name: 2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-α-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-D-glucal
• CAS No.: 1380673-18-6
• Molecular Formula: C₇₄H₇₈O₁₄
• Molecular Weight: 1191.42

Synonyms:2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-α-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-D-glucal

Chemical Property of 2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-α-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-D-glucal

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Technology Process of 2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-α-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-D-glucal

There total 1 articles about 2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-α-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-D-glucal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C59H67NO10S2 + 3,4-di-O-benzyl-D-glucal (58871-10-6) → 2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-α-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-D-glucal (1380673-18-6) + O-(2,3,4,6-Tetra-O-benzyl-β-D-glucopyranosyl)-(1->6)-O-(3,4-di-O-benzyl-β-D-glucopyranosyl)-(1->6)-1,5-anhydro-3,4-di-O-benzyl-2-deoxy-D-arabino-hex-1-enopyranose (121654-10-2)

Guidance literature:

C₅₉H₆₇NO₁₀S₂; With 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; 1,2-dichloro-ethane; at 20 ℃; for 1h; Molecular sieve;

With copper(I) triflate benzene complex; In dichloromethane; 1,2-dichloro-ethane; at -50 ℃; for 0.166667h;

3,4-di-O-benzyl-D-glucal; In dichloromethane; 1,2-dichloro-ethane; at -50 - -30 ℃; for 15.8333h; stereoselective reaction;

DOI:10.1021/ol301349w

upstream raw materials:

3,4-di-O-benzyl-D-glucal

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