N^α-(tert-butyloxycarbonyl)-L-prolyl-L-phenylalanyl-L-histidine benzyl ester

Base Information

Chemical Name:N^α-(tert-butyloxycarbonyl)-L-prolyl-L-phenylalanyl-L-histidine benzyl ester
CAS No.:132235-83-7
Molecular Formula:C₃₂H₃₉N₅O₆
Molecular Weight:589.692
Hs Code.:

N<sup>α</sup>-(tert-butyloxycarbonyl)-L-prolyl-L-phenylalanyl-L-histidine benzyl ester

Synonyms:N^α-(tert-butyloxycarbonyl)-L-prolyl-L-phenylalanyl-L-histidine benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^α-(tert-butyloxycarbonyl)-L-prolyl-L-phenylalanyl-L-histidine benzyl ester

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Technology Process of N^α-(tert-butyloxycarbonyl)-L-prolyl-L-phenylalanyl-L-histidine benzyl ester

There total 2 articles about N^α-(tert-butyloxycarbonyl)-L-prolyl-L-phenylalanyl-L-histidine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 132235-82-6
N^α-(tert-butyloxycarbonyl)-L-prolyl-L-phenylalanyl-N^im-tosyl-L-histidine benzyl ester

: 132235-83-7
N^α-(tert-butyloxycarbonyl)-L-prolyl-L-phenylalanyl-L-histidine benzyl ester

Guidance literature:: With benzotriazol-1-ol; In methanol; for 18h;
DOI:10.1021/jm00108a006

Reference yield:

: 132259-57-5
N^α-(tert-butyloxycarbonyl)-N^im-tosyl-L-histidine benzyl ester

: 132235-83-7
N^α-(tert-butyloxycarbonyl)-L-prolyl-L-phenylalanyl-L-histidine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.9 g / trifluoroacetic acid / CH₂Cl₂ / 1 h

2: diisopropylethylamine, diethylphosphoryl cyanide / CH₂Cl₂ / 18 h

3: 100 percent / 1-hydroxybenzotriazole / methanol / 18 h

With diethylphosphoryl cyanide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1021/jm00108a006