(3aR,5S,6R,7R,7aR)-6,7-Bis-benzyloxy-2-methoxy-2,5-dimethyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran

Base Information

Chemical Name:(3aR,5S,6R,7R,7aR)-6,7-Bis-benzyloxy-2-methoxy-2,5-dimethyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran
CAS No.:143394-75-6
Molecular Formula:C₂₃H₂₈O₆
Molecular Weight:400.472
Hs Code.:

Synonyms:(3aR,5S,6R,7R,7aR)-6,7-Bis-benzyloxy-2-methoxy-2,5-dimethyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran

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Chemical Property of (3aR,5S,6R,7R,7aR)-6,7-Bis-benzyloxy-2-methoxy-2,5-dimethyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran

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Technology Process of (3aR,5S,6R,7R,7aR)-6,7-Bis-benzyloxy-2-methoxy-2,5-dimethyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran

There total 6 articles about (3aR,5S,6R,7R,7aR)-6,7-Bis-benzyloxy-2-methoxy-2,5-dimethyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88818-93-3
benzyl 2,3,4-tri-O-acetyl-6-deoxy-α-L-talopyranoside

: 143394-75-6
(3aR,5S,6R,7R,7aR)-6,7-Bis-benzyloxy-2-methoxy-2,5-dimethyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran

Guidance literature:: Multi-step reaction with 6 steps

1: H₂ / 10percent Pd-C / ethyl acetate

2: pyridine

3: HBr/AcOH

4: 2,6-lutidine

5: NaOMe / methanol

6: NaH / tetrahydrofuran

With pyridine; 2,6-dimethylpyridine; hydrogen bromide; hydrogen; sodium methylate; sodium hydride; acetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethyl acetate;

Reference yield:

: 143394-73-4
Acetic acid (3aR,5S,6R,7R,7aR)-6-acetoxy-2-methoxy-2,5-dimethyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran-7-yl ester

: 143394-75-6
(3aR,5S,6R,7R,7aR)-6,7-Bis-benzyloxy-2-methoxy-2,5-dimethyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / methanol

2: NaH / tetrahydrofuran

With sodium methylate; sodium hydride; In tetrahydrofuran; methanol;

Reference yield:

: 143332-42-7
2,3,4-O-triacetyl-6-deoxy-α-L-talose

: 143394-75-6
(3aR,5S,6R,7R,7aR)-6,7-Bis-benzyloxy-2-methoxy-2,5-dimethyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine

2: HBr/AcOH

3: 2,6-lutidine

4: NaOMe / methanol

5: NaH / tetrahydrofuran

With pyridine; 2,6-dimethylpyridine; hydrogen bromide; sodium methylate; sodium hydride; acetic acid; In tetrahydrofuran; methanol;