di(1H-imidazol-2-yl)methanethione

Base Information

• Chemical Name: di(1H-imidazol-2-yl)methanethione
• CAS No.: 88681-68-9
• Molecular Formula: C₇H₆N₄S
• Molecular Weight: 178.217
• Mol file: 88681-68-9.mol

Synonyms:di(1H-imidazol-2-yl)methanethione

Chemical Property of di(1H-imidazol-2-yl)methanethione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of di(1H-imidazol-2-yl)methanethione

There total 1 articles about di(1H-imidazol-2-yl)methanethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ trans-Decalin (493-02-7) + di(1H-imidazol-2-yl)methanethione (88681-68-9)

Guidance literature:

Reference yield: 100.0%

1-(3-bromophenyl)-1-(3-fluoropyridin-4-yl)methanamine (960503-84-8) + di(1H-imidazol-2-yl)methanethione (88681-68-9) → 4-[(3-bromophenyl)(isothiocyanato)methyl]-3-fluoropyridine (960503-85-9)

Guidance literature:

In dichloromethane; at 25 ℃; for 2h;

Reference yield: 98.6%

(R)-2-aminopropan-1-ol (35320-23-1) + (E)-N'-(4-amino-2-cyanophenyl)-N,N-dimethylformimidamide (2131230-48-1) + di(1H-imidazol-2-yl)methanethione (88681-68-9) → (R,E)-N’-(2-cyano-4-(3-(1-hydroxypropyl-2-yl)thioureido)phenyl)-N,N-dimethylformamidine

Guidance literature:

(E)-N'-(4-amino-2-cyanophenyl)-N,N-dimethylformimidamide; di(1H-imidazol-2-yl)methanethione; In tetrahydrofuran; at -8 - -5 ℃; for 0.5h;

(R)-2-aminopropan-1-ol; In tetrahydrofuran; at 20 ℃;

Downstream raw materials:

(-)-5-O-(diphenyl-t-butylsilyl)-2,3-O-(thiocarbonyl)-D-ribono-1,4-lactone

4-[(3-bromophenyl)(isothiocyanato)methyl]-3-fluoropyridine

C₉H₃F₃N₂S₂

4-methylpiperazine-1-carbothioamide