Technology Process of C18H21NO2
There total 1 articles about C18H21NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium carbonate; sodium iodide;
In
N,N-dimethyl-formamide;
at 20 - 60 ℃;
for 4.5h;
DOI:10.1039/c2cc31699d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 8 h / 0 - 20 °C
2.1: isopropylmagnesium chloride / tetrahydrofuran / 0.25 h / 0 °C
2.2: 0.17 h / 0 °C
With
sodium periodate; osmium(VIII) oxide; isopropylmagnesium chloride;
In
tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1039/c2cc31699d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 8 h / 0 - 20 °C
2.1: isopropylmagnesium chloride / tetrahydrofuran / 0.25 h / 0 °C
2.2: 0.17 h / 0 °C
3.1: trifluoroacetic acid / dichloromethane / 24 h / 20 °C
With
sodium periodate; osmium(VIII) oxide; isopropylmagnesium chloride; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c2cc31699d