Technology Process of exo-6-benzoyl-1-cyanobicyclo<2.2.2>-2-octene
There total 7 articles about exo-6-benzoyl-1-cyanobicyclo<2.2.2>-2-octene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic anhydride;
In
1,4-dioxane; pyridine;
at 50 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 13 percent / hydroquinone / 24 h / 150 °C
2: sodium ethoxide / ethanol / 72 h / Ambient temperature
3: 87 percent / KOH / ethanol / 4 h / Heating
4: 100 percent / SOCl2 / CHCl3 / 3 h / Heating
5: 61 percent / gaseous NH3 / tetrahydrofuran / 144 h / Ambient temperature
6: 93 percent / trifluoroacetic anhydride / dioxane; pyridine / 3 h / 50 °C
With
potassium hydroxide; thionyl chloride; ammonia; sodium ethanolate; hydroquinone; trifluoroacetic anhydride;
In
tetrahydrofuran; 1,4-dioxane; pyridine; ethanol; chloroform;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 13 percent / hydroquinone / 24 h / 150 °C
2: sodium ethoxide / ethanol / 72 h / Ambient temperature
3: 87 percent / KOH / ethanol / 4 h / Heating
4: 100 percent / SOCl2 / CHCl3 / 3 h / Heating
5: 61 percent / gaseous NH3 / tetrahydrofuran / 144 h / Ambient temperature
6: 93 percent / trifluoroacetic anhydride / dioxane; pyridine / 3 h / 50 °C
With
potassium hydroxide; thionyl chloride; ammonia; sodium ethanolate; hydroquinone; trifluoroacetic anhydride;
In
tetrahydrofuran; 1,4-dioxane; pyridine; ethanol; chloroform;
