5-benzyloxy-4-methoxy-2-nitro-N-<2'-(2'',3'',4''-trimethoxyphenyl)ethyl>benzamide

Base Information

Chemical Name:5-benzyloxy-4-methoxy-2-nitro-N-<2'-(2'',3'',4''-trimethoxyphenyl)ethyl>benzamide
CAS No.:152715-40-7
Molecular Formula:C₂₆H₂₈N₂O₈
Molecular Weight:496.517
Hs Code.:

Synonyms:5-benzyloxy-4-methoxy-2-nitro-N-<2'-(2'',3'',4''-trimethoxyphenyl)ethyl>benzamide

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Chemical Property of 5-benzyloxy-4-methoxy-2-nitro-N-<2'-(2'',3'',4''-trimethoxyphenyl)ethyl>benzamide

Chemical Property:

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Technology Process of 5-benzyloxy-4-methoxy-2-nitro-N-<2'-(2'',3'',4''-trimethoxyphenyl)ethyl>benzamide

There total 5 articles about 5-benzyloxy-4-methoxy-2-nitro-N-<2'-(2'',3'',4''-trimethoxyphenyl)ethyl>benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3937-16-4
2-(2,3,4-trimethoxyphenyl)ethylamine

: 107915-22-0
5-benzyloxy-4-methoxy-2-nitro-benzoyl chloride

: 152715-40-7
5-benzyloxy-4-methoxy-2-nitro-N-<2'-(2'',3'',4''-trimethoxyphenyl)ethyl>benzamide

Guidance literature:: With potassium carbonate; In chloroform; water; at 18 ℃; for 24h; Yield given;

Reference yield:

: 58749-47-6
3-hydroxy-4-methoxy-6-nitrobenzaldehyde

: 152715-40-7
5-benzyloxy-4-methoxy-2-nitro-N-<2'-(2'',3'',4''-trimethoxyphenyl)ethyl>benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / potassium carbonate / dimethylformamide / 4 h / Heating

2: 78 percent / NaClO₂, H₂NSO₃H / 2-methyl-propan-2-ol; H₂O / 2 h / 18 °C

3: thionyl chloride / 1 h / Heating

4: potassium carbonate / CHCl₃; H₂O / 24 h / 18 °C

With sodium chlorite; thionyl chloride; aminosulfonic acid; potassium carbonate; In chloroform; water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 58662-50-3
2-aldehyde-4-benzyloxy-5-methoxy nitrobenzene

: 152715-40-7
5-benzyloxy-4-methoxy-2-nitro-N-<2'-(2'',3'',4''-trimethoxyphenyl)ethyl>benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaClO₂, H₂NSO₃H / 2-methyl-propan-2-ol; H₂O / 2 h / 18 °C

2: thionyl chloride / 1 h / Heating

3: potassium carbonate / CHCl₃; H₂O / 24 h / 18 °C

With sodium chlorite; thionyl chloride; aminosulfonic acid; potassium carbonate; In chloroform; water; tert-butyl alcohol;