(E)-tert-butyl (5-methoxy-2-(methoxycarbamoyl)-3-(4-methylstyryl)phenyl)carbamate

Base Information

Chemical Name:(E)-tert-butyl (5-methoxy-2-(methoxycarbamoyl)-3-(4-methylstyryl)phenyl)carbamate
CAS No.:1440754-69-7
Molecular Formula:C₂₃H₂₈N₂O₅
Molecular Weight:412.486
Hs Code.:

Synonyms:(E)-tert-butyl (5-methoxy-2-(methoxycarbamoyl)-3-(4-methylstyryl)phenyl)carbamate

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Chemical Property of (E)-tert-butyl (5-methoxy-2-(methoxycarbamoyl)-3-(4-methylstyryl)phenyl)carbamate

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Technology Process of (E)-tert-butyl (5-methoxy-2-(methoxycarbamoyl)-3-(4-methylstyryl)phenyl)carbamate

There total 7 articles about (E)-tert-butyl (5-methoxy-2-(methoxycarbamoyl)-3-(4-methylstyryl)phenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1440755-93-0
(E)-N,4-dimethoxy-2-(4-methylstyryl)benzamide

: 1440756-11-5
tert-butyl (2,4,6-trichlorobenzoyl)oxycarbamate

: 1440754-69-7
(E)-tert-butyl (5-methoxy-2-(methoxycarbamoyl)-3-(4-methylstyryl)phenyl)carbamate

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; potassium acetate; In acetonitrile; at 50 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol401209f

Reference yield:

: 622-97-9,24936-41-2
1-ethenyl-4-methylbenzene

: 1440754-69-7
(E)-tert-butyl (5-methoxy-2-(methoxycarbamoyl)-3-(4-methylstyryl)phenyl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate / methanol / 12 h / 60 °C / Inert atmosphere

2: water / ethanol / 24 h / Reflux; Inert atmosphere

3: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0 °C / Inert atmosphere

4: potassium carbonate / ethyl acetate; water / 0 - 20 °C / Inert atmosphere

5: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; potassium acetate / acetonitrile / 16 h / 50 °C / Inert atmosphere

With oxalyl dichloride; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; water; potassium acetate; cesium acetate; potassium carbonate; N,N-dimethyl-formamide; In methanol; ethanol; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1021/ol401209f

Reference yield:

: 1440755-89-4
C₁₇H₁₆O₃

: 1440754-69-7
(E)-tert-butyl (5-methoxy-2-(methoxycarbamoyl)-3-(4-methylstyryl)phenyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0 °C / Inert atmosphere

2: potassium carbonate / ethyl acetate; water / 0 - 20 °C / Inert atmosphere

3: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; potassium acetate / acetonitrile / 16 h / 50 °C / Inert atmosphere

With oxalyl dichloride; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; potassium acetate; potassium carbonate; N,N-dimethyl-formamide; In dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1021/ol401209f