Technology Process of C29H30FNO4
There total 11 articles about C29H30FNO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / methanol / 1 h / 20 °C
2.1: sodium t-butanolate / N,N-dimethyl-formamide / 1.5 h / -45 - -40 °C
2.2: -10 °C
3.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 760.05 Torr
With
palladium 10% on activated carbon; hydrogen; potassium carbonate; sodium t-butanolate;
In
methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium t-butanolate / N,N-dimethyl-formamide / 1.5 h / -45 - -40 °C
1.2: -10 °C
2.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 760.05 Torr
With
palladium 10% on activated carbon; hydrogen; sodium t-butanolate;
In
methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: thionyl chloride / 7 h / Reflux
2.1: thionyl chloride / 0.5 h / Reflux
2.2: 2 h / 0 - 20 °C
3.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C
4.1: dimethyl sulfoxide / 20 - 90 °C
5.1: potassium carbonate / methanol / 1 h / 20 °C
6.1: sodium t-butanolate / N,N-dimethyl-formamide / 1.5 h / -45 - -40 °C
6.2: -10 °C
7.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 760.05 Torr
With
thionyl chloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; sodium t-butanolate;
In
methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
