2-(Cyclohexylcarbonyl)-4-oxo-1,2,3,6,7,12b-hexahydropyrazino[1,2-d][1,4]benzoxazepine

Base Information

Chemical Name:2-(Cyclohexylcarbonyl)-4-oxo-1,2,3,6,7,12b-hexahydropyrazino[1,2-d][1,4]benzoxazepine
CAS No.:121654-76-0
Molecular Formula:C₁₉H₂₄N₂O₃
Molecular Weight:328.411
Hs Code.:

Synonyms:2-(Cyclohexylcarbonyl)-4-oxo-1,2,3,6,7,12b-hexahydropyrazino[1,2-d][1,4]benzoxazepine

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Chemical Property of 2-(Cyclohexylcarbonyl)-4-oxo-1,2,3,6,7,12b-hexahydropyrazino[1,2-d][1,4]benzoxazepine

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Technology Process of 2-(Cyclohexylcarbonyl)-4-oxo-1,2,3,6,7,12b-hexahydropyrazino[1,2-d][1,4]benzoxazepine

There total 4 articles about 2-(Cyclohexylcarbonyl)-4-oxo-1,2,3,6,7,12b-hexahydropyrazino[1,2-d][1,4]benzoxazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121654-48-6
4-Oxo-1,2,3,6,7,12b-hexahydropyrazino[1,2-d][1,4]benzoxazepine

: 121654-76-0
2-(Cyclohexylcarbonyl)-4-oxo-1,2,3,6,7,12b-hexahydropyrazino[1,2-d][1,4]benzoxazepine

Guidance literature:: With ammonium hydroxide; triethylamine; In dichloromethane; cyclohexanylcarbonyl chloride;

Reference yield:

: 98123-71-8
1-(2-phenoxyethyl)-4-benzyl-2,6-piperazinedione

: 121654-76-0
2-(Cyclohexylcarbonyl)-4-oxo-1,2,3,6,7,12b-hexahydropyrazino[1,2-d][1,4]benzoxazepine

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄, NaHCO₃ / ethanol; H₂O / 5 °C

2: polyphosphoric acid / 180 °C

3: H₂ / Pd-C / ethanol / 45 °C / 760 Torr

With sodium tetrahydroborate; PPA; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In ethanol; water;
DOI:10.1021/jm00129a007

Reference yield:

: 121654-46-4
2-benzyl-4-oxo-1,2,3,6,7,12b-hexahydropyrazino[1,2-d][1,4]benzoxazepine

: 121654-76-0
2-(Cyclohexylcarbonyl)-4-oxo-1,2,3,6,7,12b-hexahydropyrazino[1,2-d][1,4]benzoxazepine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd-C / ethanol / 45 °C / 760 Torr

With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00129a007