Technology Process of C46H52N2O8
There total 4 articles about C46H52N2O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic acid; zinc;
In
tetrahydrofuran; water;
at 60 ℃;
for 18h;
Inert atmosphere;
DOI:10.3762/bjoc.10.182
- Guidance literature:
-
Multi-step reaction with 3 steps
1: L-Selectride / tetrahydrofuran / 1 h / -10 °C / Inert atmosphere
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water; N,N-dimethyl-formamide / 48 h / 70 °C / Inert atmosphere; Sealed tube
3: zinc; acetic acid / tetrahydrofuran; water / 18 h / 60 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); L-Selectride; sodium carbonate; acetic acid; zinc;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
2: |Suzuki Coupling;
DOI:10.3762/bjoc.10.182
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1H-imidazole / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
2: L-Selectride / tetrahydrofuran / 1 h / -10 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water; N,N-dimethyl-formamide / 48 h / 70 °C / Inert atmosphere; Sealed tube
4: zinc; acetic acid / tetrahydrofuran; water / 18 h / 60 °C / Inert atmosphere
With
1H-imidazole; tetrakis(triphenylphosphine) palladium(0); L-Selectride; sodium carbonate; acetic acid; zinc;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
3: |Suzuki Coupling;
DOI:10.3762/bjoc.10.182
