2,3-di-O-acetyl-1,5-benzyloxycarbonylimino6-O-tert-butyldiphenylsilyl-1,5-dideoxy-D-glucito

Base Information

Chemical Name:2,3-di-O-acetyl-1,5-benzyloxycarbonylimino6-O-tert-butyldiphenylsilyl-1,5-dideoxy-D-glucito
CAS No.:153373-54-7
Molecular Formula:C₃₄H₄₁NO₈Si
Molecular Weight:619.787
Hs Code.:

Synonyms:2,3-di-O-acetyl-1,5-benzyloxycarbonylimino6-O-tert-butyldiphenylsilyl-1,5-dideoxy-D-glucito

Suppliers and Price of 2,3-di-O-acetyl-1,5-benzyloxycarbonylimino6-O-tert-butyldiphenylsilyl-1,5-dideoxy-D-glucito

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3-di-O-acetyl-1,5-benzyloxycarbonylimino6-O-tert-butyldiphenylsilyl-1,5-dideoxy-D-glucito

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3-di-O-acetyl-1,5-benzyloxycarbonylimino6-O-tert-butyldiphenylsilyl-1,5-dideoxy-D-glucito

There total 4 articles about 2,3-di-O-acetyl-1,5-benzyloxycarbonylimino6-O-tert-butyldiphenylsilyl-1,5-dideoxy-D-glucito which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 153373-53-6
2,3-di-O-acetyl-1,5-benzyloxycarbonylimino-1,5-dideoxy-D-glucitol

: 153373-54-7
2,3-di-O-acetyl-1,5-benzyloxycarbonylimino6-O-tert-butyldiphenylsilyl-1,5-dideoxy-D-glucito

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1016/0008-6215(95)00068-5

Reference yield: 93.0%

: 153373-54-7
2,3-di-O-acetyl-1,5-benzyloxycarbonylimino6-O-tert-butyldiphenylsilyl-1,5-dideoxy-D-glucito

Guidance literature:

Reference yield:

: 138381-83-6
4,6-O-(R-Benzylidene)-N-benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glucitol

: 153373-54-7
2,3-di-O-acetyl-1,5-benzyloxycarbonylimino6-O-tert-butyldiphenylsilyl-1,5-dideoxy-D-glucito

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine

2: 100 percent / 80percent aq. AcOH / 6 h / 45 °C

3: 93 percent / pyridine / 20 °C

With pyridine; acetic acid;
DOI:10.1016/0008-6215(95)00068-5