2-(2-methyl-4-(1-(3-(4-methyl-5-oxo-1-(4-trifluoromethyl-phenyl)-4,5-dihydrogen-1H-1,2,4-triazolyl))-benzyloxy)-phenoxy)-acetic acid

Base Information

Chemical Name:2-(2-methyl-4-(1-(3-(4-methyl-5-oxo-1-(4-trifluoromethyl-phenyl)-4,5-dihydrogen-1H-1,2,4-triazolyl))-benzyloxy)-phenoxy)-acetic acid
CAS No.:1207268-97-0
Molecular Formula:C₂₆H₂₂F₃N₃O₅
Molecular Weight:513.473
Hs Code.:

Synonyms:2-(2-methyl-4-(1-(3-(4-methyl-5-oxo-1-(4-trifluoromethyl-phenyl)-4,5-dihydrogen-1H-1,2,4-triazolyl))-benzyloxy)-phenoxy)-acetic acid

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Chemical Property of 2-(2-methyl-4-(1-(3-(4-methyl-5-oxo-1-(4-trifluoromethyl-phenyl)-4,5-dihydrogen-1H-1,2,4-triazolyl))-benzyloxy)-phenoxy)-acetic acid

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Technology Process of 2-(2-methyl-4-(1-(3-(4-methyl-5-oxo-1-(4-trifluoromethyl-phenyl)-4,5-dihydrogen-1H-1,2,4-triazolyl))-benzyloxy)-phenoxy)-acetic acid

There total 11 articles about 2-(2-methyl-4-(1-(3-(4-methyl-5-oxo-1-(4-trifluoromethyl-phenyl)-4,5-dihydrogen-1H-1,2,4-triazolyl))-benzyloxy)-phenoxy)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.5%

: 1207268-78-7
ethyl 2-(2-methyl-4-(1-(3-(4-methyl-5-oxo-1-(4-trifluoromethyl-phenyl)-4,5-dihydrogen-1H-1,2,4-triazolyl))-benzyloxy)-phenoxy)-acetate

: 1207268-97-0
2-(2-methyl-4-(1-(3-(4-methyl-5-oxo-1-(4-trifluoromethyl-phenyl)-4,5-dihydrogen-1H-1,2,4-triazolyl))-benzyloxy)-phenoxy)-acetic acid

Guidance literature:: ethyl 2-(2-methyl-4-(1-(3-(4-methyl-5-oxo-1-(4-trifluoromethyl-phenyl)-4,5-dihydrogen-1H-1,2,4-triazolyl))-benzyloxy)-phenoxy)-acetate; With sodium hydroxide; In methanol; dichloromethane; at 20 ℃; for 12h;

With hydrogenchloride; In methanol; dichloromethane; water; pH=2 - 3;

Reference yield:

: 876-02-8
4-hydroxy-3-methylphenyl methyl ketone

: 1207268-97-0
2-(2-methyl-4-(1-(3-(4-methyl-5-oxo-1-(4-trifluoromethyl-phenyl)-4,5-dihydrogen-1H-1,2,4-triazolyl))-benzyloxy)-phenoxy)-acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetonitrile / 8 h / 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / toluene-4-sulfonic acid / dichloromethane / 20 °C

3.1: ethanol / toluene-4-sulfonic acid / 6 h / Reflux

4.1: dmap; potassium carbonate / acetonitrile / 8 h / 20 °C

5.1: sodium hydroxide / dichloromethane; methanol / 12 h / 20 °C

5.2: pH 2 - 3

With dmap; ethanol; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; toluene-4-sulfonic acid; In methanol; dichloromethane; acetonitrile;

Reference yield:

: 42018-09-7
ethyl 2-(4-acetyl-2-methylphenoxy)acetate

: 1207268-97-0
2-(2-methyl-4-(1-(3-(4-methyl-5-oxo-1-(4-trifluoromethyl-phenyl)-4,5-dihydrogen-1H-1,2,4-triazolyl))-benzyloxy)-phenoxy)-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: 3-chloro-benzenecarboperoxoic acid / toluene-4-sulfonic acid / dichloromethane / 20 °C

2.1: ethanol / toluene-4-sulfonic acid / 6 h / Reflux

3.1: dmap; potassium carbonate / acetonitrile / 8 h / 20 °C

4.1: sodium hydroxide / dichloromethane; methanol / 12 h / 20 °C

4.2: pH 2 - 3

With dmap; ethanol; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; toluene-4-sulfonic acid; In methanol; dichloromethane; acetonitrile;