8-chloro-6-(2-fluoro-phenyl)-1-methyl-4-oxo-1H,6H-pyrazolo-[4,3-d]⁽²⁾benzoxepine

Base Information

• Chemical Name: 8-chloro-6-(2-fluoro-phenyl)-1-methyl-4-oxo-1H,6H-pyrazolo-[4,3-d]⁽²⁾benzoxepine
• CAS No.: 60690-96-2
• Molecular Formula: C₁₈H₁₂ClFN₂O₂
• Molecular Weight: 342.757

Synonyms:8-chloro-6-(2-fluoro-phenyl)-1-methyl-4-oxo-1H,6H-pyrazolo-[4,3-d]⁽²⁾benzoxepine

Chemical Property of 8-chloro-6-(2-fluoro-phenyl)-1-methyl-4-oxo-1H,6H-pyrazolo-[4,3-d]⁽²⁾benzoxepine

Chemical Property:

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Technology Process of 8-chloro-6-(2-fluoro-phenyl)-1-methyl-4-oxo-1H,6H-pyrazolo-[4,3-d]⁽²⁾benzoxepine

There total 1 articles about 8-chloro-6-(2-fluoro-phenyl)-1-methyl-4-oxo-1H,6H-pyrazolo-[4,3-d]⁽²⁾benzoxepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(4-chloro-2-(α-chloro-2-fluoro-benzyl)-phenyl]-4-ethoxycarbonyl-2-methyl-pyrazole + 4-carboxy-3-[4-chloro-2-(2-fluoro-α-hydroxy-benzyl)-phenyl]-2-methyl-pyrazole → 8-chloro-6-(2-fluoro-phenyl)-1-methyl-4-oxo-1H,6H-pyrazolo-[4,3-d](2)benzoxepine (60690-96-2)

Guidance literature:

With hydrogenchloride; sodium hydroxide; toluene-4-sulfonic acid; In 1,4-dioxane; toluene;

Reference yield:

8-chloro-6-(2-fluoro-phenyl)-1-methyl-4-oxo-1H,6H-pyrazolo-[4,3-d](2)benzoxepine (60690-96-2) → 3-[4-chloro-2-(2-fluoro-α-hydroxy-benzyl)-phenyl]-4-hydroxymethyl-2-methyl-pyrazole (58582-89-1)

Guidance literature:

With hydrogenchloride; sodium carbonate; In tetrahydrofuran; 1,4-dioxane; diethyl ether; sulfuric acid; water; toluene;

Downstream raw materials:

3-[4-chloro-2-(2-fluoro-α-hydroxy-benzyl)-phenyl]-4-hydroxymethyl-2-methyl-pyrazole

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