N-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzoylmethyl-4-fluoropiperidine hydrochloride

Base Information

Chemical Name:N-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzoylmethyl-4-fluoropiperidine hydrochloride
CAS No.:1064709-43-8
Molecular Formula:C₂₁H₂₂FNO₃
Molecular Weight:355.409
Hs Code.:

Synonyms:N-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzoylmethyl-4-fluoropiperidine hydrochloride

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Chemical Property of N-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzoylmethyl-4-fluoropiperidine hydrochloride

Chemical Property:

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Technology Process of N-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzoylmethyl-4-fluoropiperidine hydrochloride

There total 3 articles about N-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzoylmethyl-4-fluoropiperidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1064709-01-8
N-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzoylmethyl-4-piperidinol

: 1064709-43-8
N-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzoylmethyl-4-fluoropiperidine hydrochloride

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at -75 - -10 ℃; for 3h; Cooling with acetone-dry ice; Inert atmosphere;

Reference yield:

: 1064708-73-1
4-benzoylmethyl-4-piperidinol

: 1064709-43-8
N-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzoylmethyl-4-fluoropiperidine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 8 h / Reflux

2: diethylamino-sulfur trifluoride / dichloromethane / 3 h / -75 - -10 °C / Cooling with acetone-dry ice; Inert atmosphere

With diethylamino-sulfur trifluoride; potassium carbonate; In dichloromethane; acetone;

Reference yield:

: 2606-51-1
3,4-Methylenedioxybenzyl bromide

: 1064709-43-8
N-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzoylmethyl-4-fluoropiperidine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 8 h / Reflux

2: diethylamino-sulfur trifluoride / dichloromethane / 3 h / -75 - -10 °C / Cooling with acetone-dry ice; Inert atmosphere

With diethylamino-sulfur trifluoride; potassium carbonate; In dichloromethane; acetone;