Technology Process of C22H24O5
There total 8 articles about C22H24O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chloro-trimethyl-silane; sodium cyanoborohydride;
In
acetonitrile;
at 0 ℃;
Inert atmosphere;
Heating;
DOI:10.1021/ja203642n
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium chlorite; sodium phosphate monobasic monohydrate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 °C
2: sulfuric acid / 0 - 20 °C / Inert atmosphere
3: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere
4: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating
With
sodium chlorite; chloro-trimethyl-silane; sodium phosphate monobasic monohydrate; sulfuric acid; sodium cyanoborohydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; 2-methyl-but-2-ene; water; acetonitrile; tert-butyl alcohol;
1: Pinnick oxidation;
DOI:10.1021/ja203642n
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuric acid / 0 - 20 °C / Inert atmosphere
2: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere
3: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating
With
chloro-trimethyl-silane; sulfuric acid; sodium cyanoborohydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; acetonitrile;
DOI:10.1021/ja203642n
