C₂₈H₃₀BrN₅O₅S

Base Information

• Chemical Name: C₂₈H₃₀BrN₅O₅S
• CAS No.: 1310719-66-4
• Molecular Formula: C₂₈H₃₀BrN₅O₅S
• Molecular Weight: 628.547
• Mol file: 1310719-66-4.mol

Synonyms:C₂₈H₃₀BrN₅O₅S

Chemical Property of C₂₈H₃₀BrN₅O₅S

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₂₈H₃₀BrN₅O₅S

There total 4 articles about C₂₈H₃₀BrN₅O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-ethyl-6-bromo-5-aminosaccharin (1310720-02-5) + 3-(N-benzyl-(N-propyl)amino)-4-methoxyacetanilide (1310718-41-2) → C28H30BrN5O5S (1310719-66-4)

Guidance literature:

N-ethyl-6-bromo-5-aminosaccharin; With nitrosylsulfuric acid; sulfuric acid; In water; acetic acid; at 2 ℃; for 3.25h;

3-(N-benzyl-(N-propyl)amino)-4-methoxyacetanilide; With aminosulfonic acid; sodium hydroxide; In water; acetic acid; at 3 - 6 ℃; for 1h; pH=1.45 - 2;

Reference yield:

N-ethyl-6-bromosaccharin → C28H30BrN5O5S (1310719-66-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: nitric acid; sulfur trioxide; sulfuric acid / 28.5 h / 55 - 80 °C

1.2: Cooling with ice

2.1: hydrogenchloride; tin / water; methanol / 8 h / 75 °C

3.1: sulfuric acid; nitrosylsulfuric acid / water; acetic acid / 3.25 h / 2 °C

3.2: 1 h / 3 - 6 °C / pH 1.45 - 2

With hydrogenchloride; tin; nitrosylsulfuric acid; sulfuric acid; sulfur trioxide; nitric acid; In methanol; water; acetic acid;

Reference yield:

N-ethyl-6-bromo-5-nitrosaccharin (1310720-04-7) → C28H30BrN5O5S (1310719-66-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogenchloride; tin / water; methanol / 8 h / 75 °C

2.1: sulfuric acid; nitrosylsulfuric acid / water; acetic acid / 3.25 h / 2 °C

2.2: 1 h / 3 - 6 °C / pH 1.45 - 2

With hydrogenchloride; tin; nitrosylsulfuric acid; sulfuric acid; In methanol; water; acetic acid;

upstream raw materials:

6-bromosaccharin

N-ethyl-6-bromo-5-nitrosaccharin

N-ethyl-6-bromo-5-aminosaccharin

3-(N-benzyl-(N-propyl)amino)-4-methoxyacetanilide

Downstream raw materials:

C₂₉H₃₀N₆O₅S