5-amino-2-[2-(4,6-dimethoxypyrimidin-2-yloxy)-phenyl]-[1,3,4]thiadiazole

Base Information

Chemical Name:5-amino-2-[2-(4,6-dimethoxypyrimidin-2-yloxy)-phenyl]-[1,3,4]thiadiazole
CAS No.:1219034-57-7
Molecular Formula:C₁₄H₁₃N₅O₃S
Molecular Weight:331.355
Hs Code.:

Synonyms:5-amino-2-[2-(4,6-dimethoxypyrimidin-2-yloxy)-phenyl]-[1,3,4]thiadiazole

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Chemical Property of 5-amino-2-[2-(4,6-dimethoxypyrimidin-2-yloxy)-phenyl]-[1,3,4]thiadiazole

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Technology Process of 5-amino-2-[2-(4,6-dimethoxypyrimidin-2-yloxy)-phenyl]-[1,3,4]thiadiazole

There total 4 articles about 5-amino-2-[2-(4,6-dimethoxypyrimidin-2-yloxy)-phenyl]-[1,3,4]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 144264-09-5
C₁₄H₁₅N₅O₃S

: 1219034-57-7
5-amino-2-[2-(4,6-dimethoxypyrimidin-2-yloxy)-phenyl]-[1,3,4]thiadiazole

Guidance literature:: With iron(III) chloride hexahydrate; In methanol; for 8h; Reflux;
DOI:10.1002/jhet.1853

Reference yield:

: 110284-76-9
2-(4,6-dimethoxy-pyrimidin-2-yl-oxy)benzaldehyde

: 1219034-57-7
5-amino-2-[2-(4,6-dimethoxypyrimidin-2-yloxy)-phenyl]-[1,3,4]thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 4.5 h / 20 °C / Reflux

2: iron(III) chloride hexahydrate / methanol / 8 h / Reflux

With iron(III) chloride hexahydrate; In methanol; ethanol;
DOI:10.1002/jhet.1853

Reference yield:

: 113583-35-0
4,6-dimethoxypyrimidin-2-yl methyl sulfone

: 1219034-57-7
5-amino-2-[2-(4,6-dimethoxypyrimidin-2-yloxy)-phenyl]-[1,3,4]thiadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate

2: ethanol / 4.5 h / 20 °C / Reflux

3: iron(III) chloride hexahydrate / methanol / 8 h / Reflux

With iron(III) chloride hexahydrate; potassium carbonate; In methanol; ethanol;
DOI:10.1002/jhet.1853