benzyl 2-acetamido-2-deoxy-3,6-di-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-galactopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-2-deoxy-3,6-di-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-galactopyranoside
CAS No.:85230-50-8
Molecular Formula:C₅₅H₅₉N₃O₂₄
Molecular Weight:1146.08
Hs Code.:

Synonyms:benzyl 2-acetamido-2-deoxy-3,6-di-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-galactopyranoside

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Chemical Property of benzyl 2-acetamido-2-deoxy-3,6-di-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-galactopyranoside

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Technology Process of benzyl 2-acetamido-2-deoxy-3,6-di-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-galactopyranoside

There total 1 articles about benzyl 2-acetamido-2-deoxy-3,6-di-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.6%

: 85069-37-0
benzyl 2-acetamido-2-deoxy-3-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-galactopyranoside

: 10028-45-2
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl bromide

: 85230-50-8
benzyl 2-acetamido-2-deoxy-3,6-di-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-galactopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; for 2.5h; Ambient temperature;
DOI:10.1016/0008-6215(83)88219-6

Reference yield:

: 85230-50-8
benzyl 2-acetamido-2-deoxy-3,6-di-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-galactopyranoside

: C₃₉H₅₅N₃O₂₀

Guidance literature:: With hydrazine hydrate; In ethanol; at 70 ℃; for 0.25h;
DOI:10.1016/0008-6215(83)88219-6

Reference yield:

: 85230-50-8
benzyl 2-acetamido-2-deoxy-3,6-di-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-galactopyranoside

: 85230-52-0
benzyl 2-acetamido-3,6-di-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent hydrazine hydrate / ethanol / 0.25 h / 70 °C

2: 80.8 percent / pyridine / 0.33 h / 90 °C

3: 85.7 percent / 0.1 M sodium methoxide / methanol / 2 h / Ambient temperature

With sodium methylate; hydrazine hydrate; In pyridine; methanol; ethanol;
DOI:10.1016/0008-6215(83)88219-6