(S,E)-2,4-di-tert-butyl-6-((4-tert-butylphenyl)(1-hydroxy-3,3-dimethylbutan-2-ylimino)methyl)phenol

Base Information

Chemical Name:(S,E)-2,4-di-tert-butyl-6-((4-tert-butylphenyl)(1-hydroxy-3,3-dimethylbutan-2-ylimino)methyl)phenol
CAS No.:1438106-18-3
Molecular Formula:C₃₁H₄₇NO₂
Molecular Weight:465.72
Hs Code.:

Synonyms:(S,E)-2,4-di-tert-butyl-6-((4-tert-butylphenyl)(1-hydroxy-3,3-dimethylbutan-2-ylimino)methyl)phenol

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Chemical Property of (S,E)-2,4-di-tert-butyl-6-((4-tert-butylphenyl)(1-hydroxy-3,3-dimethylbutan-2-ylimino)methyl)phenol

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Technology Process of (S,E)-2,4-di-tert-butyl-6-((4-tert-butylphenyl)(1-hydroxy-3,3-dimethylbutan-2-ylimino)methyl)phenol

There total 3 articles about (S,E)-2,4-di-tert-butyl-6-((4-tert-butylphenyl)(1-hydroxy-3,3-dimethylbutan-2-ylimino)methyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 31314-36-0
4-tert-butylphenyl(3,5-di-tert-butyl-2-hydroxy-phenyl)methanone

: 112245-13-3
(S)-tert-leucinol

: 1438106-18-3
(S,E)-2,4-di-tert-butyl-6-((4-tert-butylphenyl)(1-hydroxy-3,3-dimethylbutan-2-ylimino)methyl)phenol

Guidance literature:: With sodium sulfate; In toluene; at 115 ℃; for 51h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tetasy.2013.03.017

Reference yield:

: 19715-19-6
3,5-ditertbutyl salicylic acid

: 1438106-18-3
(S,E)-2,4-di-tert-butyl-6-((4-tert-butylphenyl)(1-hydroxy-3,3-dimethylbutan-2-ylimino)methyl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / dichloromethane / 0.75 h / 20 °C / Inert atmosphere; Schlenk technique

1.2: 24 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: magnesium; iodine / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere; Schlenk technique

2.2: 20 h / 25 °C / Inert atmosphere; Schlenk technique

2.3: Cooling with ice; Inert atmosphere; Schlenk technique

3.1: sodium sulfate / toluene / 51 h / 115 °C / Inert atmosphere; Schlenk technique

With thionyl chloride; iodine; magnesium; sodium sulfate; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tetasy.2013.03.017

Reference yield:

: 1438105-96-4
(1H-benzo[d][1,2,3]triazol-1-yl)(3,5-di-tert-butyl-2-hydroxyphenyl)methanone

: 1438106-18-3
(S,E)-2,4-di-tert-butyl-6-((4-tert-butylphenyl)(1-hydroxy-3,3-dimethylbutan-2-ylimino)methyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium; iodine / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere; Schlenk technique

1.2: 20 h / 25 °C / Inert atmosphere; Schlenk technique

1.3: Cooling with ice; Inert atmosphere; Schlenk technique

2.1: sodium sulfate / toluene / 51 h / 115 °C / Inert atmosphere; Schlenk technique

With iodine; magnesium; sodium sulfate; In tetrahydrofuran; toluene;
DOI:10.1016/j.tetasy.2013.03.017