Valylhistidine

Base Information

• Chemical Name: Valylhistidine
• CAS No.: 13589-07-6
• Molecular Formula: C₁₁H₁₈N₄O₃
• Molecular Weight: 254.289
• Hs Code.: 2933290090
• DSSTox Substance ID: DTXSID00428629
• Nikkaji Number: J1.064.341D
• Wikidata: Q27143864
• Metabolomics Workbench ID: 79044
• Mol file: 13589-07-6.mol

Synonyms:valylhistidine;H-Val-His-OH;Val-His;13589-07-6;L-valyl-L-histidine;(2S)-2-[[(2S)-2-amino-3-methylbutanoyl]amino]-3-(1H-imidazol-5-yl)propanoic acid;(2S)-2-[[(2S)-2-azaniumyl-3-methylbutanoyl]amino]-3-(1H-imidazol-5-yl)propanoate;L-Histidine, L-valyl-;valyl-histidine;VH dipeptide;V-H Dipeptide;L-Val-L-His;Valine Histidine dipeptide;Valine-Histidine dipeptide;SCHEMBL78174;CHEBI:73700;DTXSID00428629;HY-P4666;MFCD00238272;AKOS010421286;CS-0655749;J-006781;Q27143864;(S)-2-((S)-2-Amino-3-methylbutanamido)-3-(1H-imidazol-4-yl)propanoic acid;V-H

Chemical Property of Valylhistidine

Chemical Property:

• PSA: 121.10000
• LogP: 0.59610
• Storage Temp.: -15°C
• Solubility.: Methanol. Water
• XLogP3: -2.5
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 6
• Exact Mass: 254.13789045
• Heavy Atom Count: 18
• Complexity: 309

Purity/Quality:

98%Min ^*data from raw suppliers

L-Valyl-L-histidine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)C(C(=O)NC(CC1=CN=CN1)C(=O)O)N
• Isomeric SMILES: CC(C)[C@@H](C(=O)N[C@@H](CC1=CN=CN1)C(=O)O)N
• Uses: L-Valyl-L-histidine, is used to synthesize Glu-Val-His (I) by reacting it with glucose in pyridine and AcOH.

Technology Process of Valylhistidine

There total 5 articles about Valylhistidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ Val-His (13589-07-6)

Guidance literature:

With water; hydrogen bromide; acetic acid;

DOI:10.1002/hlca.19580410512

Reference yield:

→ Nα-Ξ-valyl-L-histidine (13589-07-6,51077-04-4,51077-05-5,51077-07-7,51077-08-8,51077-09-9,51077-10-2,51077-11-3)

Guidance literature:

With ammonia; water;

Reference yield:

Val-His-Leu-Thr-Pro-Val-Glu-Lys → Leu-Thr-Pro-Val-Glu-Lys + Val-His (13589-07-6)

Guidance literature:

With ammonium acetate; dipeptidyl aminopeptidase I; 2-mercaptoethylamine hydrochloride; at 27 ℃; digesting investigated;

DOI:10.1002/oms.1210220516

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