C₁₄H₁₈Br₃NO₃

Base Information

Chemical Name:C₁₄H₁₈Br₃NO₃
CAS No.:1359715-02-8
Molecular Formula:C₁₄H₁₈Br₃NO₃
Molecular Weight:488.014
Hs Code.:

C<sub>14</sub>H<sub>18</sub>Br<sub>3</sub>NO<sub>3</sub>

Synonyms:C₁₄H₁₈Br₃NO₃

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Chemical Property of C₁₄H₁₈Br₃NO₃

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Technology Process of C₁₄H₁₈Br₃NO₃

There total 6 articles about C₁₄H₁₈Br₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1359715-00-6
2-(2,3,4-tribromo-5-methoxyphenyl)ethanamine hydrochloride

: 1359715-02-8
C₁₄H₁₈Br₃NO₃

Guidance literature:: With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; at 0 - 20 ℃;
DOI:10.1021/jo3000173

Reference yield:

: 1359714-96-7
2,3,4-tribromo-5-methoxybenzaldehyde

: 1359715-02-8
C₁₄H₁₈Br₃NO₃

Guidance literature:: Multi-step reaction with 5 steps

1: ammonium acetate / 5 h / Reflux

2: borane-dimethyl sulfide complex / tetrahydrofuran / 0.33 h / 0 °C

3: sodium tetrahydroborate / tetrahydrofuran / 156 h / 20 °C

4: hydrogenchloride / 1,4-dioxane; chloroform

5: sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; water / 0 - 20 °C

With hydrogenchloride; sodium tetrahydroborate; borane-dimethyl sulfide complex; ammonium acetate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; chloroform; water;
DOI:10.1021/jo3000173

Reference yield:

: 1359715-20-0
C₈H₇Br₃O₂

: 1359715-02-8
C₁₄H₁₈Br₃NO₃

Guidance literature:: Multi-step reaction with 6 steps

1: pyridinium chlorochromate / dichloromethane / 60 h / 0 - 20 °C

2: ammonium acetate / 5 h / Reflux

3: borane-dimethyl sulfide complex / tetrahydrofuran / 0.33 h / 0 °C

4: sodium tetrahydroborate / tetrahydrofuran / 156 h / 20 °C

5: hydrogenchloride / 1,4-dioxane; chloroform

6: sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; water / 0 - 20 °C

With hydrogenchloride; sodium tetrahydroborate; borane-dimethyl sulfide complex; ammonium acetate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; chloroform; water;
DOI:10.1021/jo3000173