N,N,N'-tris((tert-butoxycarbonyl)methyl)-N'-(2-((triphenylmethyl)amino)ethyl)-1,2-ethanediamine

Base Information

• Chemical Name: N,N,N'-tris((tert-butoxycarbonyl)methyl)-N'-(2-((triphenylmethyl)amino)ethyl)-1,2-ethanediamine
• CAS No.: 163687-65-8
• Molecular Formula: C₄₁H₅₇N₃O₆
• Molecular Weight: 687.92
• Mol file: 163687-65-8.mol

Synonyms:N,N,N'-tris((tert-butoxycarbonyl)methyl)-N'-(2-((triphenylmethyl)amino)ethyl)-1,2-ethanediamine

Chemical Property of N,N,N'-tris((tert-butoxycarbonyl)methyl)-N'-(2-((triphenylmethyl)amino)ethyl)-1,2-ethanediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N,N'-tris((tert-butoxycarbonyl)methyl)-N'-(2-((triphenylmethyl)amino)ethyl)-1,2-ethanediamine

There total 2 articles about N,N,N'-tris((tert-butoxycarbonyl)methyl)-N'-(2-((triphenylmethyl)amino)ethyl)-1,2-ethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

bromoacetic acid tert-butyl ester (5292-43-3) + N-(2-(triphenylmethyl)amino)ethyl-1,2-ethanediamine → N,N,N'-tris((tert-butoxycarbonyl)methyl)-N'-(2-((triphenylmethyl)amino)ethyl)-1,2-ethanediamine (163687-65-8)

Guidance literature:

With caesium carbonate; In acetonitrile; at 4 ℃; for 12h;

DOI:10.1021/jo00125a062

Reference yield:

trityl chloride (76-83-5) → N,N,N'-tris((tert-butoxycarbonyl)methyl)-N'-(2-((triphenylmethyl)amino)ethyl)-1,2-ethanediamine (163687-65-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / CH₂Cl₂ / 0 °C

2: 77 percent / Cs₂CO₃ / acetonitrile / 12 h / 4 °C

With caesium carbonate; In dichloromethane; acetonitrile;

DOI:10.1021/jo00125a062

upstream raw materials:

bromoacetic acid tert-butyl ester

trityl chloride