2-[⁽²⁾-6-[(4-Methylphenyl)sulfonyloxy]-6-(phenylseleno)-5-hexenyl] 1,3-dioxoisoindoline

Base Information

• Chemical Name: 2-[⁽²⁾-6-[(4-Methylphenyl)sulfonyloxy]-6-(phenylseleno)-5-hexenyl] 1,3-dioxoisoindoline
• CAS No.: 350508-72-4
• Molecular Formula: C₂₇H₂₅NO₅SSe
• Molecular Weight: 554.525

Synonyms:2-[⁽²⁾-6-[(4-Methylphenyl)sulfonyloxy]-6-(phenylseleno)-5-hexenyl] 1,3-dioxoisoindoline

Chemical Property of 2-[⁽²⁾-6-[(4-Methylphenyl)sulfonyloxy]-6-(phenylseleno)-5-hexenyl] 1,3-dioxoisoindoline

Chemical Property:

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Technology Process of 2-[⁽²⁾-6-[(4-Methylphenyl)sulfonyloxy]-6-(phenylseleno)-5-hexenyl] 1,3-dioxoisoindoline

There total 3 articles about 2-[⁽²⁾-6-[(4-Methylphenyl)sulfonyloxy]-6-(phenylseleno)-5-hexenyl] 1,3-dioxoisoindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

toluene-4-sulfonic acid (104-15-4) + 2-(6-phenylselanyl-hex-5-ynyl)-isoindole-1,3-dione (350508-86-0) → 2-[(2)-6-[(4-Methylphenyl)sulfonyloxy]-6-(phenylseleno)-5-hexenyl] 1,3-dioxoisoindoline (350508-72-4)

Guidance literature:

In dichloromethane; at 40 - 50 ℃;

DOI:10.1055/s-2001-13370

Reference yield:

2-(hex-5-yn-1-yl)isoindole-1,3-dione (6097-08-1) → 2-[(2)-6-[(4-Methylphenyl)sulfonyloxy]-6-(phenylseleno)-5-hexenyl] 1,3-dioxoisoindoline (350508-72-4)

Guidance literature:

Multi-step reaction with 2 steps

1: PhI(OAc)2

2: 74 percent / CH₂Cl₂ / 40 - 50 °C

With [bis(acetoxy)iodo]benzene; In dichloromethane;

DOI:10.1055/s-2001-13370

Reference yield:

diphenyl diselenide (1666-13-3) → 2-[(2)-6-[(4-Methylphenyl)sulfonyloxy]-6-(phenylseleno)-5-hexenyl] 1,3-dioxoisoindoline (350508-72-4)

Guidance literature:

Multi-step reaction with 2 steps

1: PhI(OAc)2

2: 74 percent / CH₂Cl₂ / 40 - 50 °C

With [bis(acetoxy)iodo]benzene; In dichloromethane;

DOI:10.1055/s-2001-13370

upstream raw materials:

toluene-4-sulfonic acid

2-(6-phenylselanyl-hex-5-ynyl)-isoindole-1,3-dione

2-(hex-5-yn-1-yl)isoindole-1,3-dione

diphenyl diselenide

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