C₂₃H₂₀ClNSi

Base Information

Chemical Name:C₂₃H₂₀ClNSi
CAS No.:1359766-63-4
Molecular Formula:C₂₃H₂₀ClNSi
Molecular Weight:373.957
Hs Code.:

Synonyms:C₂₃H₂₀ClNSi

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Chemical Property of C₂₃H₂₀ClNSi

Chemical Property:

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Technology Process of C₂₃H₂₀ClNSi

There total 5 articles about C₂₃H₂₀ClNSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1299410-89-1
C₂₃H₂₁BrClNSi

: 1359766-63-4
C₂₃H₂₀ClNSi

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; tetrabutylammomium bromide; sodium t-butanolate; In toluene; at 120 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c2ob06941e

Reference yield:

: 31928-44-6
2-bromo-4-chloroiodobenzene

: 1359766-63-4
C₂₃H₂₀ClNSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: zirconocene dichloride / diethyl ether; toluene / 2 h / 0 °C / Inert atmosphere

2.2: 12 h / 0 - 100 °C / Inert atmosphere

2.3: 12 h / 0 - 20 °C / Inert atmosphere

3.1: palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / toluene / 10 h / 120 °C / Inert atmosphere

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; tetrabutylammomium bromide; sodium t-butanolate / toluene / 12 h / 120 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; zirconocene dichloride; tri-tert-butyl phosphine; tetrabutylammomium bromide; palladium diacetate; caesium carbonate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1039/c2ob06941e

Reference yield:

: 2-bromo-4-chloro-1-[2-(trimethylsilyl)ethynyl]benzene

: 1359766-63-4
C₂₃H₂₀ClNSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: zirconocene dichloride / diethyl ether; toluene / 2 h / 0 °C / Inert atmosphere

1.2: 12 h / 0 - 100 °C / Inert atmosphere

1.3: 12 h / 0 - 20 °C / Inert atmosphere

2.1: palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene / toluene / 10 h / 120 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; tetrabutylammomium bromide; sodium t-butanolate / toluene / 12 h / 120 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; zirconocene dichloride; tri-tert-butyl phosphine; tetrabutylammomium bromide; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; sodium t-butanolate; In diethyl ether; toluene;
DOI:10.1039/c2ob06941e