C₃₁H₄₆O₇

Base Information

Chemical Name:C₃₁H₄₆O₇
CAS No.:950598-43-3
Molecular Formula:C₃₁H₄₆O₇
Molecular Weight:530.702
Hs Code.:

C<sub>31</sub>H<sub>46</sub>O<sub>7</sub>

Synonyms:C₃₁H₄₆O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₄₆O₇

Chemical Property:

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Technology Process of C₃₁H₄₆O₇

There total 25 articles about C₃₁H₄₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 950598-32-0
(2E,5S,5R,7R,9Z,11S,14E)-7,11-epoxy-5,6-(isopropylidenedioxy)-16-(4-methoxybenzyloxy)-2,6,10,14-tetramethylhexadeca-2,9,14-trien-1-ol

: 950598-43-3
C₃₁H₄₆O₇

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate; 4 A molecular sieve; In dichloromethane; at -40 ℃; for 17h;
DOI:10.1021/ja073952e

Reference yield: 95.0%

: C₃₁H₄₆O₆

: 950598-43-3
C₃₁H₄₆O₇

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate; In dichloromethane; at -40 ℃; for 17h; Molecular sieve; Inert atmosphere;
DOI:10.1021/jo802249k

Reference yield:

: 906624-11-1
(3S,6E)-8-(4-methoxybenzyloxy)-2,6-dimethylocta-1,6-dien-3-ol

: 950598-43-3
C₃₁H₄₆O₇

Guidance literature:: Multi-step reaction with 16 steps

1: 97 percent / DCC; DMAP / CH₂Cl₂ / 0 °C

2: 74 percent / [RuCl₂(=CHPh)(PCy₃)(SIMes)] / CH₂Cl₂ / 40 °C

3: DIBALH / CH₂Cl₂ / -78 °C

4: toluene / 80 °C

5: imidazole / CH₂Cl₂

6: DIBALH / CH₂Cl₂ / -78 °C

7: L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / -20 °C

8: SO₃*pyridine; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

9: 63 percent / LDA / diethyl ether / -78 °C

10: imidazole / CH₂Cl₂

11: DIBALH / CH₂Cl₂ / -78 °C

12: toluene / 80 °C

13: DIBALH / CH₂Cl₂ / -78 °C

14: 97 percent / BF₃*OEt₂ / methanol / 3 h / -78 - 0 °C

15: 91 percent / PPTS / CH₂Cl₂ / 1 h / 20 °C

16: 95 percent / L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / 17 h / -40 °C

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; pyridine-SO₃ complex; diethyl (2R,3R)-tartrate; boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; 4 A molecular sieve; In methanol; diethyl ether; dichloromethane; toluene; 4: Wittig reaction / 7: Sharpless asymmetric epoxidation / 12: Wittig reaction / 16: Sharpless asymmetric epoxidation;
DOI:10.1021/ja073952e