allyl 3,4,5-tri(acetyloxy)-6-([4-([1-(tert-butyl)-1,1-dimethylsilyl]oxymethyl)anilino]carbonyloxy)tetrahydro-2H-2-pyrancarboxylate

Base Information

Chemical Name:allyl 3,4,5-tri(acetyloxy)-6-([4-([1-(tert-butyl)-1,1-dimethylsilyl]oxymethyl)anilino]carbonyloxy)tetrahydro-2H-2-pyrancarboxylate
CAS No.:1184951-80-1
Molecular Formula:C₃₇H₄₈N₂O₁₄Si
Molecular Weight:772.879
Hs Code.:

Synonyms:allyl 3,4,5-tri(acetyloxy)-6-([4-([1-(tert-butyl)-1,1-dimethylsilyl]oxymethyl)anilino]carbonyloxy)tetrahydro-2H-2-pyrancarboxylate

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Chemical Property of allyl 3,4,5-tri(acetyloxy)-6-([4-([1-(tert-butyl)-1,1-dimethylsilyl]oxymethyl)anilino]carbonyloxy)tetrahydro-2H-2-pyrancarboxylate

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Technology Process of allyl 3,4,5-tri(acetyloxy)-6-([4-([1-(tert-butyl)-1,1-dimethylsilyl]oxymethyl)anilino]carbonyloxy)tetrahydro-2H-2-pyrancarboxylate

There total 1 articles about allyl 3,4,5-tri(acetyloxy)-6-([4-([1-(tert-butyl)-1,1-dimethylsilyl]oxymethyl)anilino]carbonyloxy)tetrahydro-2H-2-pyrancarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1184951-79-8
allyl 3,4,5-tri(acetyloxy)-6-([4-(hydroxymethyl)anilino]carbonyloxy)tetrahydro-2H-2-pyrancarboxylate

: 922173-23-7
tert-butyl[(4-isocyanatophenyl)methoxy]dimethylsilane

: 1184951-80-1
allyl 3,4,5-tri(acetyloxy)-6-([4-([1-(tert-butyl)-1,1-dimethylsilyl]oxymethyl)anilino]carbonyloxy)tetrahydro-2H-2-pyrancarboxylate

Guidance literature:: In toluene; for 18h;

Reference yield: 44.0%

: 1184951-80-1
allyl 3,4,5-tri(acetyloxy)-6-([4-([1-(tert-butyl)-1,1-dimethylsilyl]oxymethyl)anilino]carbonyloxy)tetrahydro-2H-2-pyrancarboxylate

: 107-19-7
propargyl alcohol

: 2-propynyl 3,4,5-trihydroxy-6-[([4-(hydroxymethyl)anilino]carbonyl)oxy]tetrahydro-2H-2-pyrancarboxylate

Guidance literature:: propargyl alcohol; With sodium;

allyl 3,4,5-tri(acetyloxy)-6-([4-([1-(tert-butyl)-1,1-dimethylsilyl]oxymethyl)anilino]carbonyloxy)tetrahydro-2H-2-pyrancarboxylate; for 1.5h;

With potassium hydrogensulfate; In water; pH=< 7;