C₃₆H₄₄ClNO₄Si

Base Information

Chemical Name:C₃₆H₄₄ClNO₄Si
CAS No.:880152-44-3
Molecular Formula:C₃₆H₄₄ClNO₄Si
Molecular Weight:618.288
Hs Code.:

C<sub>36</sub>H<sub>44</sub>ClNO<sub>4</sub>Si

Synonyms:C₃₆H₄₄ClNO₄Si

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Chemical Property of C₃₆H₄₄ClNO₄Si

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Technology Process of C₃₆H₄₄ClNO₄Si

There total 15 articles about C₃₆H₄₄ClNO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: C₃₆H₄₆ClNO₄Si

: 880152-44-3
C₃₆H₄₄ClNO₄Si

Guidance literature:: With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ol053059p

Reference yield:

: 880152-30-7
2-(3-tert-butoxycarbonylamino-4-hydroxy-butyl)-cyclohex-1-enecarboxylic acid ethyl ester

: 880152-44-3
C₃₆H₄₄ClNO₄Si

Guidance literature:: Multi-step reaction with 10 steps

1: imidazole / CH₂Cl₂ / 20 °C

2: 12.0 g / DIBAL-H / CH₂Cl₂ / -78 - 0 °C

3: pyridine / 20 °C

4: 100 percent / TFA / CH₂Cl₂ / 1 h / 0 °C

5: 61 percent / pyridine / ethanol / 48 h / Heating

6: K₂CO₃ / methanol; H₂O / 1 h / 20 °C

7: 504.0 mg / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h / 20 °C

8: 68 percent / Na₂SO₄; piperidinium acetate / ethyl acetate; toluene / Heating

9: 76 percent / N-chlorosuccinimide; H₂O / 2-methyl-propan-2-ol / 1 h / 20 °C

10: 66 percent / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 4 h / 20 °C

With pyridine; 1H-imidazole; N-chloro-succinimide; tetrapropylammonium perruthennate; 4 A molecular sieve; water; piperdinium acetate; diisobutylaluminium hydride; potassium carbonate; 4-methylmorpholine N-oxide; sodium sulfate; trifluoroacetic acid; In methanol; ethanol; dichloromethane; water; ethyl acetate; toluene; tert-butyl alcohol;

Reference yield:

: 6-butyl-4-[1-(tert-butyl-diphenyl-silanyloxymethyl)-3-(2-hydroxymethyl-cyclohex-1-enyl)-propylamino]-pyran-2-one

: 880152-44-3
C₃₆H₄₄ClNO₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: 504.0 mg / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h / 20 °C

2: 68 percent / Na₂SO₄; piperidinium acetate / ethyl acetate; toluene / Heating

3: 76 percent / N-chlorosuccinimide; H₂O / 2-methyl-propan-2-ol / 1 h / 20 °C

4: 66 percent / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 4 h / 20 °C

With N-chloro-succinimide; tetrapropylammonium perruthennate; 4 A molecular sieve; water; piperdinium acetate; 4-methylmorpholine N-oxide; sodium sulfate; In dichloromethane; ethyl acetate; toluene; tert-butyl alcohol;