2-[(N-benzyloxycarbonyl)amino]ethyl 3,4-cyclic sulfite-6-deoxy-β-D-galactopyranoside

Base Information

Chemical Name:2-[(N-benzyloxycarbonyl)amino]ethyl 3,4-cyclic sulfite-6-deoxy-β-D-galactopyranoside
CAS No.:1314864-85-1
Molecular Formula:C₁₆H₂₁NO₈S
Molecular Weight:387.411
Hs Code.:

Synonyms:2-[(N-benzyloxycarbonyl)amino]ethyl 3,4-cyclic sulfite-6-deoxy-β-D-galactopyranoside

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Chemical Property of 2-[(N-benzyloxycarbonyl)amino]ethyl 3,4-cyclic sulfite-6-deoxy-β-D-galactopyranoside

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Technology Process of 2-[(N-benzyloxycarbonyl)amino]ethyl 3,4-cyclic sulfite-6-deoxy-β-D-galactopyranoside

There total 5 articles about 2-[(N-benzyloxycarbonyl)amino]ethyl 3,4-cyclic sulfite-6-deoxy-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₃NO₇

: 1314864-85-1
2-[(N-benzyloxycarbonyl)amino]ethyl 3,4-cyclic sulfite-6-deoxy-β-D-galactopyranoside

Guidance literature:: With thionyl chloride; triethylamine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/jo200340q

Reference yield:

: 77987-49-6
benzyl 2-hydroxyethylcarbamate

: 1314864-84-0
1,2:3,4-bis-cyclic sulfite-6-deoxy-β-D-galactopyranose

: 1314864-85-1
2-[(N-benzyloxycarbonyl)amino]ethyl 3,4-cyclic sulfite-6-deoxy-β-D-galactopyranoside

: 1314864-86-2
C₁₆H₂₁NO₈S

Guidance literature:: 1,2:3,4-bis-cyclic sulfite-6-deoxy-β-D-galactopyranose; With ytterbium(III) triflate; In toluene; for 0.5h; Molecular sieve; Inert atmosphere;

benzyl 2-hydroxyethylcarbamate; at 100 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jo200340q

Reference yield:

: 6189-71-5
α-D-fucose

: 1314864-85-1
2-[(N-benzyloxycarbonyl)amino]ethyl 3,4-cyclic sulfite-6-deoxy-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole; thionyl chloride / tetrahydrofuran / 2 h / -20 °C / Inert atmosphere

2.1: ytterbium(III) triflate / toluene / 0.5 h / Molecular sieve; Inert atmosphere

2.2: 4 h / 100 °C / Inert atmosphere

With 1H-imidazole; thionyl chloride; ytterbium(III) triflate; In tetrahydrofuran; toluene;
DOI:10.1021/jo200340q