(2H,2H,4H,4H,-3,6,9,12-tetraoxaperfluorohexadecanoic acid)N-{2-[1-O-α-d-(2,3,4,6-tetra-O-benzyl)mannopyranosyl]ethyl}amide

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Chemical Name:(2H,2H,4H,4H,-3,6,9,12-tetraoxaperfluorohexadecanoic acid)N-{2-[1-O-α-d-(2,3,4,6-tetra-O-benzyl)mannopyranosyl]ethyl}amide
CAS No.:1020857-57-1
Molecular Formula:C₄₈H₄₄F₁₉NO₁₁
Molecular Weight:1171.85
Hs Code.:

Synonyms:(2H,2H,4H,4H,-3,6,9,12-tetraoxaperfluorohexadecanoic acid)N-{2-[1-O-α-d-(2,3,4,6-tetra-O-benzyl)mannopyranosyl]ethyl}amide

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Chemical Property of (2H,2H,4H,4H,-3,6,9,12-tetraoxaperfluorohexadecanoic acid)N-{2-[1-O-α-d-(2,3,4,6-tetra-O-benzyl)mannopyranosyl]ethyl}amide

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Technology Process of (2H,2H,4H,4H,-3,6,9,12-tetraoxaperfluorohexadecanoic acid)N-{2-[1-O-α-d-(2,3,4,6-tetra-O-benzyl)mannopyranosyl]ethyl}amide

There total 4 articles about (2H,2H,4H,4H,-3,6,9,12-tetraoxaperfluorohexadecanoic acid)N-{2-[1-O-α-d-(2,3,4,6-tetra-O-benzyl)mannopyranosyl]ethyl}amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1020856-93-2
2H,2H,4H,4H,-3,6,9,12-tetraoxaperfluorohexadecanoic acid

: 705951-24-2
2-[1-O-α-d-(2,3,4,6-tetra-O-benzyl)mannopyranosyl]ethylamine

: 1020857-57-1
(2H,2H,4H,4H,-3,6,9,12-tetraoxaperfluorohexadecanoic acid)N-{2-[1-O-α-d-(2,3,4,6-tetra-O-benzyl)mannopyranosyl]ethyl}amide

Guidance literature:: With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 19h;

Reference yield:

: 317817-24-6
1H,1H-perfluoro-3,6,9-trioxatridecan-1-ol

: 1020857-57-1
(2H,2H,4H,4H,-3,6,9,12-tetraoxaperfluorohexadecanoic acid)N-{2-[1-O-α-d-(2,3,4,6-tetra-O-benzyl)mannopyranosyl]ethyl}amide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / tetra(n-butyl)ammonium hydrogensulfate / toluene / 14 h / 0 - 20 °C

2: sodium hydroxide; water / methanol / 12 h / 60 °C

3: 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 19 h / 0 - 20 °C

With potassium hydroxide; sodium hydroxide; 1-hydroxy-pyrrolidine-2,5-dione; water; dicyclohexyl-carbodiimide; tetra(n-butyl)ammonium hydrogensulfate; In methanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: C₁₆H₁₃F₁₉O₆

: 1020857-57-1
(2H,2H,4H,4H,-3,6,9,12-tetraoxaperfluorohexadecanoic acid)N-{2-[1-O-α-d-(2,3,4,6-tetra-O-benzyl)mannopyranosyl]ethyl}amide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / methanol / 12 h / 60 °C

2: 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 19 h / 0 - 20 °C

With sodium hydroxide; 1-hydroxy-pyrrolidine-2,5-dione; water; dicyclohexyl-carbodiimide; In methanol; N,N-dimethyl-formamide;