(Z)-8-(tetrahydro-2H-pyran-2-yloxy)oct-4-enyl 4-methylbenzensulfonate

Base Information

Chemical Name:(Z)-8-(tetrahydro-2H-pyran-2-yloxy)oct-4-enyl 4-methylbenzensulfonate
CAS No.:108536-01-2
Molecular Formula:C₂₀H₃₀O₅S
Molecular Weight:382.521
Hs Code.:

Synonyms:(Z)-8-(tetrahydro-2H-pyran-2-yloxy)oct-4-enyl 4-methylbenzensulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-8-(tetrahydro-2H-pyran-2-yloxy)oct-4-enyl 4-methylbenzensulfonate

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Technology Process of (Z)-8-(tetrahydro-2H-pyran-2-yloxy)oct-4-enyl 4-methylbenzensulfonate

There total 3 articles about (Z)-8-(tetrahydro-2H-pyran-2-yloxy)oct-4-enyl 4-methylbenzensulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 62422-46-2
(Z)-8-<(tetrahydropyran-2-yl)oxy>oct-4-enol

: 98-59-9
p-toluenesulfonyl chloride

: 108536-01-2
(Z)-8-(tetrahydro-2H-pyran-2-yloxy)oct-4-enyl 4-methylbenzensulfonate

Guidance literature:: With pyridine; at 20 ℃; for 4h;
DOI:10.5012/bkcs.2011.32.8.3120

Reference yield:

: 1552-12-1,111-78-4
1,5-cis,cis-cyclooctadiene

: 108536-01-2
(Z)-8-(tetrahydro-2H-pyran-2-yloxy)oct-4-enyl 4-methylbenzensulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: peracetic acid / dichloromethane

2: pyridinium p-toluenesulfonate / tetrahydrofuran

3: pyridine / 4 h / 20 °C

With pyridine; peracetic acid; pyridinium p-toluenesulfonate; In tetrahydrofuran; dichloromethane;
DOI:10.5012/bkcs.2011.32.8.3120

Reference yield:

: 56506-08-2,62422-45-1
(Z)-oct-4-ene-1,8-diol

: 108536-01-2
(Z)-8-(tetrahydro-2H-pyran-2-yloxy)oct-4-enyl 4-methylbenzensulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / tetrahydrofuran

2: pyridine / 4 h / 20 °C

With pyridine; pyridinium p-toluenesulfonate; In tetrahydrofuran;
DOI:10.5012/bkcs.2011.32.8.3120