ethyl 2-(2-aminothiazol-4-yl)-2-<(Z)-<2-<(2-nitrophenyl)seleno>ethoxy>imino>acetate

Base Information

Chemical Name:ethyl 2-(2-aminothiazol-4-yl)-2-<(Z)-<2-<(2-nitrophenyl)seleno>ethoxy>imino>acetate
CAS No.:139306-42-6
Molecular Formula:C₁₅H₁₆N₄O₅SSe
Molecular Weight:443.342
Hs Code.:

Synonyms:ethyl 2-(2-aminothiazol-4-yl)-2-<(Z)-<2-<(2-nitrophenyl)seleno>ethoxy>imino>acetate

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Chemical Property of ethyl 2-(2-aminothiazol-4-yl)-2-<(Z)-<2-<(2-nitrophenyl)seleno>ethoxy>imino>acetate

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Technology Process of ethyl 2-(2-aminothiazol-4-yl)-2-<(Z)-<2-<(2-nitrophenyl)seleno>ethoxy>imino>acetate

There total 5 articles about ethyl 2-(2-aminothiazol-4-yl)-2-<(Z)-<2-<(2-nitrophenyl)seleno>ethoxy>imino>acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51694-22-5
ortho-nitrophenyl selenocyanate

: 139306-42-6
ethyl 2-(2-aminothiazol-4-yl)-2-<(Z)-<2-<(2-nitrophenyl)seleno>ethoxy>imino>acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / Bu₃P / tetrahydrofuran / 0.25 h / Ambient temperature

2: 1.) CF₃SO₃SiMe₃, Et₃N, 2.) NBS / 1.) CH₂Cl₂, r.t., 0.5 h, 2.) 0.5 h

3: PhNMe₂ / ethanol / 2 h / Ambient temperature

With N-Bromosuccinimide; tributylphosphine; trimethylsilyl trifluoromethanesulfonate; N,N-dimethyl-aniline; triethylamine; In tetrahydrofuran; ethanol;

Reference yield:

: 66508-93-8
ethyl 2-(hydroxyimino)-3-oxybutyrate

: 139306-42-6
ethyl 2-(2-aminothiazol-4-yl)-2-<(Z)-<2-<(2-nitrophenyl)seleno>ethoxy>imino>acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / K₂CO₃ / dimethylformamide / 17 h / Ambient temperature

2: 86 percent / Bu₃P / tetrahydrofuran / 0.25 h / Ambient temperature

3: 1.) CF₃SO₃SiMe₃, Et₃N, 2.) NBS / 1.) CH₂Cl₂, r.t., 0.5 h, 2.) 0.5 h

4: PhNMe₂ / ethanol / 2 h / Ambient temperature

With N-Bromosuccinimide; tributylphosphine; trimethylsilyl trifluoromethanesulfonate; potassium carbonate; N,N-dimethyl-aniline; triethylamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 139306-40-4
ethyl 2-<(2-hydroxyethoxy)imino>-3-oxobutanoate

: 139306-42-6
ethyl 2-(2-aminothiazol-4-yl)-2-<(Z)-<2-<(2-nitrophenyl)seleno>ethoxy>imino>acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / Bu₃P / tetrahydrofuran / 0.25 h / Ambient temperature

2: 1.) CF₃SO₃SiMe₃, Et₃N, 2.) NBS / 1.) CH₂Cl₂, r.t., 0.5 h, 2.) 0.5 h

3: PhNMe₂ / ethanol / 2 h / Ambient temperature

With N-Bromosuccinimide; tributylphosphine; trimethylsilyl trifluoromethanesulfonate; N,N-dimethyl-aniline; triethylamine; In tetrahydrofuran; ethanol;