2,4,6-Trichloro-3,5-dinitrotrifluoromethylsulfonylbenzene

Base Information

Chemical Name:2,4,6-Trichloro-3,5-dinitrotrifluoromethylsulfonylbenzene
CAS No.:220826-34-6
Molecular Formula:C₇Cl₃F₃N₂O₆S
Molecular Weight:403.507
Hs Code.:

Synonyms:2,4,6-Trichloro-3,5-dinitrotrifluoromethylsulfonylbenzene

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Chemical Property of 2,4,6-Trichloro-3,5-dinitrotrifluoromethylsulfonylbenzene

Chemical Property:

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Technology Process of 2,4,6-Trichloro-3,5-dinitrotrifluoromethylsulfonylbenzene

There total 5 articles about 2,4,6-Trichloro-3,5-dinitrotrifluoromethylsulfonylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63572-10-1
3,5-Dinitrotrifluoromethylsulfonylbenzene

: 220826-34-6
2,4,6-Trichloro-3,5-dinitrotrifluoromethylsulfonylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 21 percent / NaHS / methanol / 0.5 h / Heating

2: 76 percent / HCl, H₂O, H₂O₂ / acetic acid / 1.) 3.5 h, 2.) reflux, overnight

3: H₂O₂, H₂O, trifluoroacetic anhydride / 1.) 0 deg C, 4 h, 2.) r.t., overnight

With hydrogenchloride; sodium hydrogensulfide; water; dihydrogen peroxide; trifluoroacetic anhydride; In methanol; acetic acid;
DOI:10.1002/(SICI)1521-3765(19990104)5:1<29::AID-CHEM29>3.0.CO;2-5

Reference yield:

: 6276-04-6
3,5-dinitroiodobenzene

: 220826-34-6
2,4,6-Trichloro-3,5-dinitrotrifluoromethylsulfonylbenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / dimethylformamide

2: 85.1 percent / CrO₃, TFAA, H₂SO₄ / Ambient temperature

3: 21 percent / NaHS / methanol / 0.5 h / Heating

4: 76 percent / HCl, H₂O, H₂O₂ / acetic acid / 1.) 3.5 h, 2.) reflux, overnight

5: H₂O₂, H₂O, trifluoroacetic anhydride / 1.) 0 deg C, 4 h, 2.) r.t., overnight

With chromium(VI) oxide; hydrogenchloride; sodium hydrogensulfide; sulfuric acid; water; dihydrogen peroxide; trifluoroacetic anhydride; In methanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1521-3765(19990104)5:1<29::AID-CHEM29>3.0.CO;2-5

Reference yield:

: 220826-26-6
1,3-dinitro-5-(trifluoromethylthio)benzene

: 220826-34-6
2,4,6-Trichloro-3,5-dinitrotrifluoromethylsulfonylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 85.1 percent / CrO₃, TFAA, H₂SO₄ / Ambient temperature

2: 21 percent / NaHS / methanol / 0.5 h / Heating

3: 76 percent / HCl, H₂O, H₂O₂ / acetic acid / 1.) 3.5 h, 2.) reflux, overnight

4: H₂O₂, H₂O, trifluoroacetic anhydride / 1.) 0 deg C, 4 h, 2.) r.t., overnight

With chromium(VI) oxide; hydrogenchloride; sodium hydrogensulfide; sulfuric acid; water; dihydrogen peroxide; trifluoroacetic anhydride; In methanol; acetic acid;
DOI:10.1002/(SICI)1521-3765(19990104)5:1<29::AID-CHEM29>3.0.CO;2-5