1-[5-(4-methoxyphenyl)-2-methylthien-3-yl]-2,3,3,4,4,5,5-heptafluorocyclopentene

Base Information

Chemical Name:1-[5-(4-methoxyphenyl)-2-methylthien-3-yl]-2,3,3,4,4,5,5-heptafluorocyclopentene
CAS No.:169030-74-4
Molecular Formula:C₁₇H₁₁F₇OS
Molecular Weight:396.329
Hs Code.:

Synonyms:1-[5-(4-methoxyphenyl)-2-methylthien-3-yl]-2,3,3,4,4,5,5-heptafluorocyclopentene

Suppliers and Price of 1-[5-(4-methoxyphenyl)-2-methylthien-3-yl]-2,3,3,4,4,5,5-heptafluorocyclopentene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-[5-(4-methoxyphenyl)-2-methylthien-3-yl]-2,3,3,4,4,5,5-heptafluorocyclopentene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-[5-(4-methoxyphenyl)-2-methylthien-3-yl]-2,3,3,4,4,5,5-heptafluorocyclopentene

There total 5 articles about 1-[5-(4-methoxyphenyl)-2-methylthien-3-yl]-2,3,3,4,4,5,5-heptafluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 559-40-0
octaperfluorocyclopentene

: 156686-75-8
3-bromo-5-(4-methoxyphenyl)-2-methylthiophene

: 169030-74-4
1-[5-(4-methoxyphenyl)-2-methylthien-3-yl]-2,3,3,4,4,5,5-heptafluorocyclopentene

Guidance literature:: 3-bromo-5-(4-methoxyphenyl)-2-methylthiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -70 ℃; for 1h;

octaperfluorocyclopentene; In tetrahydrofuran; hexane; at -70 ℃; for 3h;
DOI:10.1016/S0040-4020(03)01141-4

Reference yield:

: 154566-69-5
3-bromo-2-methylthiophene-5-boronic acid

: 169030-74-4
1-[5-(4-methoxyphenyl)-2-methylthien-3-yl]-2,3,3,4,4,5,5-heptafluorocyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate

2: n-butyllithium / -78 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; sodium carbonate;
DOI:10.1016/j.tet.2011.04.023

Reference yield:

: 554-14-3
2-Methylthiophene

: 169030-74-4
1-[5-(4-methoxyphenyl)-2-methylthien-3-yl]-2,3,3,4,4,5,5-heptafluorocyclopentene

Guidance literature:: Multi-step reaction with 4 steps

1: bromine

2: n-butyllithium / -78 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate

4: n-butyllithium / -78 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; bromine; sodium carbonate;
DOI:10.1016/j.tet.2011.04.023