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Technology Process of Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H2O)2

Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H2O)2

Base Information
  • Chemical Name:Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H2O)2
  • CAS No.:1620969-66-5
  • Molecular Formula:C28H28MnN8O8S2
  • Molecular Weight:723.649
  • Hs Code.:
Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H<SUB>2</SUB>O)<SUB>2</SUB>

Synonyms:Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H2O)2

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Chemical Property of Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H2O)2
Chemical Property:
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Technology Process of Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H2O)2

There total 2 articles about Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H2O)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine

N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine

water
7732-18-5

water

manganese(ll) chloride
7773-01-5

manganese(ll) chloride

Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H<SUB>2</SUB>O)<SUB>2</SUB>
1620969-66-5

Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H2O)2

Guidance literature:
In ethanol; at 60 ℃; for 1h; Reflux;
DOI:10.1016/j.molstruc.2014.05.078

Reference yield:

5-(4-sulfanilamidophenyl)azosalicylaldehyde

5-(4-sulfanilamidophenyl)azosalicylaldehyde

Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H<SUB>2</SUB>O)<SUB>2</SUB>
1620969-66-5

Mn(N,N'-bis(5-(4-sulfanilamidophenylazosalicylidene))ethylenediamine-(2H))(H2O)2

Guidance literature:
Multi-step reaction with 2 steps
1: ethanol / 2 h / Reflux
2: ethanol / 1 h / 60 °C / Reflux
In ethanol;
DOI:10.1016/j.molstruc.2014.05.078
upstream raw materials:

water

manganese(ll) chloride

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