methyl 3-p-hydroxyphenyl-2-t-butyldimethylsiloxy propionate

Base Information

Chemical Name:methyl 3-p-hydroxyphenyl-2-t-butyldimethylsiloxy propionate
CAS No.:481072-51-9
Molecular Formula:C₁₆H₂₆O₄Si
Molecular Weight:310.466
Hs Code.:

Synonyms:methyl 3-p-hydroxyphenyl-2-t-butyldimethylsiloxy propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-p-hydroxyphenyl-2-t-butyldimethylsiloxy propionate

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Technology Process of methyl 3-p-hydroxyphenyl-2-t-butyldimethylsiloxy propionate

There total 2 articles about methyl 3-p-hydroxyphenyl-2-t-butyldimethylsiloxy propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 481072-85-9
methyl 3-p-benzyloxyphenyl-2-t-butyldimethylsiloxy propionate

: 481072-51-9
methyl 3-p-hydroxyphenyl-2-t-butyldimethylsiloxy propionate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/j.tet.2005.06.022

Reference yield:

: 128316-64-3,481072-37-1
(+/-)-methyl 3-p-benzyloxyphenyl-2-hydroxypropionate

: 481072-51-9
methyl 3-p-hydroxyphenyl-2-t-butyldimethylsiloxy propionate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / imidazole; 4-(dimethylamino)pyridine / dimethylformamide

2: 87 percent / hydrogen / Pd/C / ethyl acetate

With 1H-imidazole; dmap; hydrogen; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2005.06.022