1,1-dimethylethyl [(4-{[2,4-bis(methyloxy)phenyl]methyl}-9-methyl-3-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-5-yl)carbonyl](4-nitrophenyl)carbamate

Base Information

Chemical Name:1,1-dimethylethyl [(4-{[2,4-bis(methyloxy)phenyl]methyl}-9-methyl-3-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-5-yl)carbonyl](4-nitrophenyl)carbamate
CAS No.:1067226-99-6
Molecular Formula:C₃₁H₃₃N₃O₉
Molecular Weight:591.618
Hs Code.:

1,1-dimethylethyl [(4-{[2,4-bis(methyloxy)phenyl]methyl}-9-methyl-3-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-5-yl)carbonyl](4-nitrophenyl)carbamate

Synonyms:1,1-dimethylethyl [(4-{[2,4-bis(methyloxy)phenyl]methyl}-9-methyl-3-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-5-yl)carbonyl](4-nitrophenyl)carbamate

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Chemical Property of 1,1-dimethylethyl [(4-{[2,4-bis(methyloxy)phenyl]methyl}-9-methyl-3-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-5-yl)carbonyl](4-nitrophenyl)carbamate

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Technology Process of 1,1-dimethylethyl [(4-{[2,4-bis(methyloxy)phenyl]methyl}-9-methyl-3-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-5-yl)carbonyl](4-nitrophenyl)carbamate

There total 6 articles about 1,1-dimethylethyl [(4-{[2,4-bis(methyloxy)phenyl]methyl}-9-methyl-3-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-5-yl)carbonyl](4-nitrophenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24589-92-2
2-(2-formyl-6-methylphenoxy)acetic acid

: 1067226-99-6
1,1-dimethylethyl [(4-{[2,4-bis(methyloxy)phenyl]methyl}-9-methyl-3-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-5-yl)carbonyl](4-nitrophenyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; methanol / 20 °C

2: dmap / acetonitrile; tetrahydrofuran / 1 h / 20 °C

With dmap; In tetrahydrofuran; methanol; acetonitrile; 1: Ugi Condensation;

Reference yield:

: 824-42-0
2-methoxy-3-methylbenzaldehyde

: 1067226-99-6
1,1-dimethylethyl [(4-{[2,4-bis(methyloxy)phenyl]methyl}-9-methyl-3-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-5-yl)carbonyl](4-nitrophenyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 60 °C

2.1: sodium hydroxide; methanol / 4 h / 20 °C

2.2: pH 2

3.1: tetrahydrofuran; methanol / 20 °C

4.1: dmap / acetonitrile; tetrahydrofuran / 1 h / 20 °C

With methanol; dmap; potassium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile; 3.1: Ugi Condensation;

Reference yield:

: 24582-03-4
methyl [(2-formyl-6-methylphenyl)oxy]acetate

: 1067226-99-6
1,1-dimethylethyl [(4-{[2,4-bis(methyloxy)phenyl]methyl}-9-methyl-3-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-5-yl)carbonyl](4-nitrophenyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; methanol / 4 h / 20 °C

1.2: pH 2

2.1: tetrahydrofuran; methanol / 20 °C

3.1: dmap / acetonitrile; tetrahydrofuran / 1 h / 20 °C

With methanol; dmap; sodium hydroxide; In tetrahydrofuran; methanol; acetonitrile; 2.1: Ugi Condensation;