1,15-bis-{3-[1-(3,3-diphenylpropyl)thioureado]}-4,12-[N-(tert-butyl)oxycarbonyl]-4,12-diazapentadecane

Base Information

• Chemical Name: 1,15-bis-{3-[1-(3,3-diphenylpropyl)thioureado]}-4,12-[N-(tert-butyl)oxycarbonyl]-4,12-diazapentadecane
• CAS No.: 1234495-35-2
• Molecular Formula: C₅₅H₇₈N₆O₄S₂
• Molecular Weight: 951.394

Synonyms:1,15-bis-{3-[1-(3,3-diphenylpropyl)thioureado]}-4,12-[N-(tert-butyl)oxycarbonyl]-4,12-diazapentadecane

Chemical Property of 1,15-bis-{3-[1-(3,3-diphenylpropyl)thioureado]}-4,12-[N-(tert-butyl)oxycarbonyl]-4,12-diazapentadecane

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Technology Process of 1,15-bis-{3-[1-(3,3-diphenylpropyl)thioureado]}-4,12-[N-(tert-butyl)oxycarbonyl]-4,12-diazapentadecane

There total 1 articles about 1,15-bis-{3-[1-(3,3-diphenylpropyl)thioureado]}-4,12-[N-(tert-butyl)oxycarbonyl]-4,12-diazapentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3,3-diphenylpropyl isothiocyanate (32265-78-4) + N1,N7-di(tert-butyloxycarbonyl)-N1,N7-di(3-aminopropyl)-1,7-heptanediamine (207552-03-2) → 1,15-bis-{3-[1-(3,3-diphenylpropyl)thioureado]}-4,12-[N-(tert-butyl)oxycarbonyl]-4,12-diazapentadecane (1234495-35-2)

Guidance literature:

In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jm100217a

Reference yield: 92.0%

1,15-bis-{3-[1-(3,3-diphenylpropyl)thioureado]}-4,12-[N-(tert-butyl)oxycarbonyl]-4,12-diazapentadecane (1234495-35-2) → 1,15-bis-{3-[1-(3,3-diphenylpropyl)thioureado]}-4,12-diazapentadecane dihydrochloride

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1021/jm100217a

upstream raw materials:

3,3-diphenylpropyl isothiocyanate

N¹,N⁷-di(tert-butyloxycarbonyl)-N¹,N⁷-di(3-aminopropyl)-1,7-heptanediamine

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