2-methyl-6-(4-(phenylmethyl)-1H-1,2,3-triazol-1-yl)pyridine

Base Information

Chemical Name:2-methyl-6-(4-(phenylmethyl)-1H-1,2,3-triazol-1-yl)pyridine
CAS No.:1224886-21-8
Molecular Formula:C₁₅H₁₄N₄
Molecular Weight:250.303
Hs Code.:

Synonyms:2-methyl-6-(4-(phenylmethyl)-1H-1,2,3-triazol-1-yl)pyridine

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Chemical Property of 2-methyl-6-(4-(phenylmethyl)-1H-1,2,3-triazol-1-yl)pyridine

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Technology Process of 2-methyl-6-(4-(phenylmethyl)-1H-1,2,3-triazol-1-yl)pyridine

There total 2 articles about 2-methyl-6-(4-(phenylmethyl)-1H-1,2,3-triazol-1-yl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 6624-45-9
5-methyltetrazolo[1,5-a]pyridine

: 10147-11-2
propargyl benzene

: 1224886-21-8
2-methyl-6-(4-(phenylmethyl)-1H-1,2,3-triazol-1-yl)pyridine

Guidance literature:: With copper(I) trifluoromethanesulfonate benzene; In toluene; at 100 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol100745d

Reference yield:

: 5315-25-3
2-bromo-6-methylpyridine

: 1224886-21-8
2-methyl-6-(4-(phenylmethyl)-1H-1,2,3-triazol-1-yl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / dimethyl sulfoxide / 20 h / 120 °C

2: copper(II) sulfate; sodium L-ascorbate; sodium hydrogencarbonate / N,N-dimethyl-formamide; water / 18 h / 20 - 100 °C

With sodium azide; sodium L-ascorbate; sodium hydrogencarbonate; copper(II) sulfate; In water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.12.008

Reference yield: 22.0%

: 50998-17-9
6-bromoquinoxaline

: 1224886-21-8
2-methyl-6-(4-(phenylmethyl)-1H-1,2,3-triazol-1-yl)pyridine

: 1422465-20-0
C₂₃H₁₈N₆

Guidance literature:: With tetrabutylammonium acetate; palladium diacetate; In 1-methyl-pyrrolidin-2-one; at 100 ℃; for 22h;
DOI:10.1016/j.bmcl.2012.12.008