13-Aminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

Base Information

Chemical Name:13-Aminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane
CAS No.:147688-16-2
Molecular Formula:C₁₂H₂₆N₂O₄
Molecular Weight:262.349
Hs Code.:

Synonyms:13-Aminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

Suppliers and Price of 13-Aminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 13-Aminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 13-Aminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

There total 1 articles about 13-Aminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 147688-16-2
13-Aminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide; tetrabutylammomium bromide / water; toluene / 10 h / 70 °C / Inert atmosphere

2: acetic acid; palladium on activated charcoal; hydrogen / methanol / 12 h / 20 °C / 7500.75 Torr / Autoclave; Inert atmosphere

3: acetonitrile; toluene / 24 h / Reflux; Inert atmosphere

4: palladium on activated charcoal; hydrogen / methanol / 20 °C / Inert atmosphere

With palladium on activated charcoal; tetrabutylammomium bromide; hydrogen; acetic acid; sodium hydroxide; In methanol; water; toluene; acetonitrile;
DOI:10.1039/c9dt01512d