C₃₀H₃₃NO₆Se

Base Information

Chemical Name:C₃₀H₃₃NO₆Se
CAS No.:96502-74-8
Molecular Formula:C₃₀H₃₃NO₆Se
Molecular Weight:582.555
Hs Code.:

C<sub>30</sub>H<sub>33</sub>NO<sub>6</sub>Se

Synonyms:C₃₀H₃₃NO₆Se

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Chemical Property of C₃₀H₃₃NO₆Se

Chemical Property:

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Technology Process of C₃₀H₃₃NO₆Se

There total 11 articles about C₃₀H₃₃NO₆Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96502-73-7
Acetic acid (1R,9S,9aS)-9-benzyloxymethyl-5,7-dimethoxy-6-methyl-1-phenylselanyl-2,3,9,9a-tetrahydro-1H-pyrrolo[1,2-a]indol-8-yl ester

: 96502-74-8
C₃₀H₃₃NO₆Se

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/ja00299a022

Reference yield:

: 2568-24-3
2-phenyl-4,7-dihydro-1,3-dioxepine

: 96502-74-8
C₃₀H₃₃NO₆Se

Guidance literature:: Multi-step reaction with 10 steps

1: LiAlH₄, AlCl₃ / diethyl ether / 1.) 0 deg C to RT, 30 min; 2.) 2 h

2: pyridinium chlorochromate, Celite / CH₂Cl₂ / 3 h

3: trimethyl borate, Zn / tetrahydrofuran / 6 h

4: LiAlH₄ / diethyl ether / 0.25 h

5: 80 percent / 4-dimethylaminopyridine, triethylamine / CH₂Cl₂ / 16 h / Ambient temperature

7: 1.) Hg(OAc)2, 90 percent HNO₃; 2.) conc. HCl, Zn / 1.) Ac₂O, glacial AcOH, 0 deg C, 5 min; 2.) methanol, 25 deg C, 15 min

8: CBr₄, triphenylphosphine / CH₂Cl₂; diethyl ether / 0.5 h / 25 °C

9: 2.) 0.5 N aq. NaOH / 1.) CH₂Cl₂, 40 min; 2.) ether

10: 85 percent MCPBA / CH₂Cl₂

With hydrogenchloride; dmap; sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; Trimethyl borate; carbon tetrabromide; Celite; mercury(II) diacetate; nitric acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; pyridinium chlorochromate; zinc; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja00299a022

Reference yield:

: 69152-87-0
4-benzyloxycrotonaldehyde

: 96502-74-8
C₃₀H₃₃NO₆Se

Guidance literature:: Multi-step reaction with 8 steps

1: trimethyl borate, Zn / tetrahydrofuran / 6 h

2: LiAlH₄ / diethyl ether / 0.25 h

3: 80 percent / 4-dimethylaminopyridine, triethylamine / CH₂Cl₂ / 16 h / Ambient temperature

5: 1.) Hg(OAc)2, 90 percent HNO₃; 2.) conc. HCl, Zn / 1.) Ac₂O, glacial AcOH, 0 deg C, 5 min; 2.) methanol, 25 deg C, 15 min

6: CBr₄, triphenylphosphine / CH₂Cl₂; diethyl ether / 0.5 h / 25 °C

7: 2.) 0.5 N aq. NaOH / 1.) CH₂Cl₂, 40 min; 2.) ether

8: 85 percent MCPBA / CH₂Cl₂

With hydrogenchloride; dmap; sodium hydroxide; lithium aluminium tetrahydride; Trimethyl borate; carbon tetrabromide; mercury(II) diacetate; nitric acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; zinc; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja00299a022