C₄₉H₇₇N₅O₁₄

Base Information

Chemical Name:C₄₉H₇₇N₅O₁₄
CAS No.:497832-43-6
Molecular Formula:C₄₉H₇₇N₅O₁₄
Molecular Weight:960.175
Hs Code.:

C<sub>49</sub>H<sub>77</sub>N<sub>5</sub>O<sub>14</sub>

Synonyms:C₄₉H₇₇N₅O₁₄

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Chemical Property of C₄₉H₇₇N₅O₁₄

Chemical Property:

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Technology Process of C₄₉H₇₇N₅O₁₄

There total 10 articles about C₄₉H₇₇N₅O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 497832-42-5
C₄₅H₇₅N₃O₁₃

: 530-62-1
1,1'-carbonyldiimidazole

: 497832-43-6
C₄₉H₇₇N₅O₁₄

Guidance literature:: In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2012.08.007

Reference yield:

: 1395892-95-1
C₅₃H₈₂N₂O₁₆

: 497832-43-6
C₄₉H₇₇N₅O₁₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: methanol / 18 h / Reflux

2.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C

3.1: lead(IV) tetraacetate / chloroform / 0.25 h / 0 °C

4.1: sodium tris(acetoxy)borohydride / chloroform / 4 h / 20 °C

5.1: sodium tris(acetoxy)borohydride / chloroform; water / 1 h / 20 °C

6.1: water; lithium hydroxide monohydrate / tetrahydrofuran; ethanol / 6 h / 20 °C

7.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 20 °C

7.2: 0.5 h / Reflux

8.1: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / 20 °C

9.1: acetone / 6 h / 20 °C

10.1: N,N-dimethyl-formamide; tetrahydrofuran / 2 h / 20 °C

With 1H-imidazole; lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; water; lead(IV) tetraacetate; sodium tris(acetoxy)borohydride; pyridine hydrogenfluoride; triethylamine; In tetrahydrofuran; methanol; ethanol; chloroform; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2012.08.007

Reference yield:

erythromycylamine: 26116-56-3
erythromycylamine

: 497832-43-6
C₄₉H₇₇N₅O₁₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydrogencarbonate / chloroform; water / 1 h / 0 °C

2.1: methanol / 18 h / Reflux

3.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C

4.1: lead(IV) tetraacetate / chloroform / 0.25 h / 0 °C

5.1: sodium tris(acetoxy)borohydride / chloroform / 4 h / 20 °C

6.1: sodium tris(acetoxy)borohydride / chloroform; water / 1 h / 20 °C

7.1: water; lithium hydroxide monohydrate / tetrahydrofuran; ethanol / 6 h / 20 °C

8.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 20 °C

8.2: 0.5 h / Reflux

9.1: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / 20 °C

10.1: acetone / 6 h / 20 °C

11.1: N,N-dimethyl-formamide; tetrahydrofuran / 2 h / 20 °C

With 1H-imidazole; lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; water; lead(IV) tetraacetate; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; pyridine hydrogenfluoride; triethylamine; In tetrahydrofuran; methanol; ethanol; chloroform; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2012.08.007